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Effect of Storage Time on Microtensile Bond Strength of Self-Adhesive and Multi-Step Resin Cements to Dentin

机译:储存时间对自粘和多步树脂胶与牙本质微拉伸粘合强度的影响

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The purpose of this study was to evaluate the effects of long-term storage on the microtensile bond strength (?μTBS) to dentin of two self-adhesive and three multi-step resin cements. Two self-adhesive cements RelyX U100 (U100) and seT PP (SET), and 3 multi-step resin cements, one using 2-step etch-and-rinse adhesive AllCem (ALC), and two conventional resin cements with self-etching primer Panavia F (PAN) and Multilink (MULT) were used. Human molars were restored (n=5), sectioned and subjected to the ??TBS test after 24 h and 6 months. Fractured specimens were examined by stereomicroscope and SEM. The ?μTBS were analyzed by one-way ANOVA and Tukey test (?±=0.05). ANOVA revealed a difference between groups (p<0.0001). All multi-step resin cements ALC, MULT and PAN showed statistically similar bond strength values that were higher than those of the U100 and SET groups. The bond strength value of ALC, MULT and PAN decreases significantly after 6 months. The majority of the failures were adhesive for all the groups. The ?μTBS produced by the self-adhesive cements were significantly lower than those observed for multi-step luting agents. Regardless of the numbers of steps of resin cements, the storage time reduces ?μTBS values to dentin only to multi-step luting agents.
机译:这项研究的目的是评估长期储存对两种自粘和三种多步树脂胶粘剂与牙本质的微拉伸粘合强度(?μTBS)的影响。两种RelyX U100(U100)和seT PP(SET)自粘胶粘剂,以及3种多步树脂胶粘剂,一种使用两步蚀刻和冲洗粘合剂AllCem(ALC),以及两种采用自蚀刻的常规树脂胶粘剂使用了底漆Panavia F(PAN)和Multilink(MULT)。在24小时和6个月后,将人的磨牙恢复(n = 5),切片并进行ΔTBS测试。通过立体显微镜和SEM检查断裂的样品。通过单向方差分析和Tukey检验(?±= 0.05)分析?μTBS。方差分析显示各组之间存在差异(p <0.0001)。所有的多步树脂胶粘剂ALC,MULT和PAN的统计强度相似,均高于U100和SET组。 6个月后,ALC,MULT和PAN的粘合强度值显着降低。对于所有组而言,大多数失败都是粘着的。自粘水泥产生的?μTBS显着低于多步浸润剂所观察到的。无论树脂胶凝剂的步骤数如何,仅在多步型浸润剂的作用下,储存时间都会使?μTBS值降低至牙本质。

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