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Effect of Aging Treatment on the Electrochemical and Corrosion Behavior of NiTiRe Shape Memory Alloy

机译:时效处理对NiTiRe形状记忆合金电化学和腐蚀行为的影响

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In this study, Ni52Ti47.7Re0.3 shape memory alloy was subjected to solution treatment at 1000 C for24h (the tested alloy), followed by ageing at 300, 400, 500 and 600 C for 3h. The objective is toinvestigate the effect of ageing temperature on the uniform and pitting corrosion characteristics ofNi52Ti47.7Re0.3 alloy. Measurements were conducted in 1.0 M H2SO4 solutions without and with 0.2 MNH4F, using polarization, impedance, and chronoamperometry measurements. Morphologies of thecorroded surfaces were examined by SEM/EDX examinations. Results obtained from the employedelectrochemical techniques were in good agreement and showed that the rates of the uniform andpitting corrosion processes of the tested alloy decrease with increase in the aging temperature, reachingo their minimum values at an aging temperature of 400 C. Further increase in the aging temperature upo to 600 C led to an obvious increase in the rates of corrosion. Experimental finding were interpretedadopting the effect of the aging temperature on the microstructure of the tested alloy.
机译:在这项研究中,Ni52Ti47.7Re0.3形状记忆合金在1000℃(测试合金)中进行了固溶处理24h,然后在300、400、500和600 C下进行了3h时效处理。目的是研究时效温度对Ni52Ti47.7Re0.3合金均匀和点蚀性能的影响。使用极化,阻抗和计时电流法测量,在没有和有0.2 MNH4F的1.0 M H2SO4溶液中进行测量。通过SEM / EDX检查来检查被腐蚀表面的形态。从采用的电化学技术获得的结果吻合良好,表明随着时效温度的升高,被测合金的均匀腐蚀和点蚀过程的速率降低,在时效温度为400 C时达到其最小值。时效进一步提高温度高达600°C导致腐蚀速率明显增加。采用时效温度对被测合金微观结构的影响来解释实验结果。

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