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A Dispersive Inelastic X-ray Scattering Spectrometer for Use at X-ray Free Electron Lasers

机译:用于X射线自由电子激光器的色散非弹性X射线散射光谱仪

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We report on the application of a short working distance von Hamos geometry spectrometer to measure the inelastic X-ray scattering (IXS) signals from solids and liquids. In contrast to typical IXS instruments where the spectrometer geometry is fixed and the incoming beam energy is scanned, the von Hamos geometry allows measurements to be made using a fixed optical arrangement with no moving parts. Thanks to the shot-to-shot capability of the spectrometer setup, we anticipate its application for the IXS technique at X-ray free electron lasers (XFELs). We discuss the capability of the spectrometer setup for IXS studies in terms of efficiency and required total incident photon flux for a given signal-to-noise ratio. The ultimate energy resolution of the spectrometer, which is a key parameter for IXS studies, was measured to the level of 150 meV at short crystal radius thanks to the application of segmented crystals for X-ray diffraction. The short working distance is a key parameter for spectrometer efficiency that is necessary to measure weak IXS signals.
机译:我们报告了一个短工作距离von Hamos几何光谱仪在测量来自固体和液体的非弹性X射线散射(IXS)信号方面的应用。与固定光谱仪几何形状并扫描入射光束能量的典型IXS仪器相比,冯·哈莫斯几何形状允许使用没有移动部件的固定光学装置进行测量。得益于分光光度计设置的逐次拍摄功能,我们预计其将在IXS技术中应用于X射线自由电子激光器(XFEL)。我们将针对给定的信噪比,在效率和所需的总入射光子通量方面,讨论用于IXS研究的光谱仪设置的功能。光谱仪的最终能量分辨率是IXS研究的关键参数,由于在X射线衍射中使用了分段晶体,因此在短晶体半径下测量的光谱仪的最终能量分辨率为150 meV。短工作距离是光谱仪效率的关键参数,这是测量弱IXS信号所必需的。

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