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Laser and Electron Beam Additive Manufacturing Methods of Fabricating Titanium Bone Implants

机译:钛骨植入物的激光和电子束增材制造方法

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摘要

Additive Manufacturing (AM) methods are generally used to produce an early sample or near net-shape elements based on three-dimensional geometrical modules. To date, publications on AM of metal implants have mainly focused on knee and hip replacements or bone scaffolds for tissue engineering. The direct fabrication of metallic implants can be achieved by methods, such as Selective Laser Melting (SLM) or Electron Beam Melting (EBM). This work compares the SLM and EBM methods used in the fabrication of titanium bone implants by analyzing the microstructure, mechanical properties and cytotoxicity. The SLM process was conducted in an environmental chamber using 0.4–0.6 vol % of oxygen to enhance the mechanical properties of a Ti-6Al-4V alloy. SLM processed material had high anisotropy of mechanical properties and superior UTS (1246–1421 MPa) when compared to the EBM (972–976 MPa) and the wrought material (933–942 MPa). The microstructure and phase composition depended on the used fabrication method. The AM methods caused the formation of long epitaxial grains of the prior β phase. The equilibrium phases (α + β) and non-equilibrium α’ martensite was obtained after EBM and SLM, respectively. Although it was found that the heat transfer that occurs during the layer by layer generation of the component caused aluminum content deviations, neither methods generated any cytotoxic effects. Furthermore, in contrast to SLM, the EBM fabricated material met the ASTMF136 standard for surgical implant applications.
机译:增材制造(AM)方法通常用于基于三维几何模块来生产早期样品或接近最终形状的元素。迄今为止,有关金属植入物的增材制造的出版物主要集中在膝关节和髋关节置换术或组织工程用的骨支架上。金属植入物的直接制造可以通过诸如选择性激光熔化(SLM)或电子束熔化(EBM)之类的方法来实现。这项工作通过分析微观结构,机械性能和细胞毒性,比较了用于制造钛骨植入物的SLM和EBM方法。 SLM工艺在环境室内进行,使用0.4-0.6%(体积)的氧气来增强Ti-6Al-4V合金的机械性能。与EBM(972-976 MPa)和锻造材料(933-942 MPa)相比,经SLM处理的材料具有较高的机械各向异性,并具有卓越的UTS(1246-1421 MPa)。微观结构和相组成取决于所使用的制造方法。 AM方法导致了先前β相的长外延晶粒的形成。 EBM和SLM后分别获得了平衡相(α+β)和非平衡α'马氏体。尽管已经发现在逐层生成组件的过程中发生的热传递会导致铝含量的偏差,但两种方法均未产生任何细胞毒性作用。此外,与SLM相比,EBM制造的材料符合用于外科植入物应用的ASTMF136标准。

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