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Saraca indica bark extract mediated green synthesis of polyshaped gold nanoparticles and its application in catalytic reduction

机译:萨拉卡in树皮提取物介导的多形金纳米粒子的绿色合成及其在催化还原中的应用

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The bark extract of the traditional ayurvedic medicinal plant Saraca indica containing redox active polyphenolic compounds has been utilized for the one-step synthesis of gold nanoparticles at room temperature. The polyphenolic compounds acted as the reducing agent as well as the stabilizing agent without any additional capping agent. The synthesis of the gold nanoparticles of 15–23?nm size was complete in several minutes and no photo irradiation or heat treatment was necessary. Surface plasmon resonance, HRTEM, AFM, X-ray diffraction, and FTIR studies have been carried out to characterize the nanoparticles. Gold nanoparticles synthesized were of triangular, tetragonal, pentagonal, hexagonal, and spherical shapes. The synthesized gold nanoparticles have been used as a catalyst for the reduction of 4-nitrophenol to 4-aminophenol at room temperature and the kinetics of the reduction reaction has been studied spectrophotometrically.
机译:含有氧化还原活性多酚化合物的传统印度草药植物萨拉卡ca的树皮提取物已用于室温下金纳米粒子的一步合成。多酚化合物充当还原剂以及稳定剂,而没有任何额外的封端剂。 15–23?nm大小的金纳米颗粒的合成在几分钟内完成,并且不需要光照射或热处理。已经进行了表面等离子体共振,HRTEM,AFM,X射线衍射和FTIR研究以表征纳米粒子。合成的金纳米颗粒具有三角形,四边形,五边形,六边形和球形。合成的金纳米粒子已被用作在室温下将4-硝基苯酚还原为4-氨基苯酚的催化剂,并且已通过分光光度法研究了还原反应的动力学。

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