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Study the Lattice Distortion and Particle Size of One Phase of MnO by Using Fourier Analysis of X-ray Diffraction Lines

机译:X射线衍射线的傅里叶分析研究MnO一相的晶格畸变和粒径

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In this study, the Fourier analysis method was used for the analysis of the X-ray diffraction pattern of MnO (111), (200), (220), (311) and (222). The particle size of each X-ray line was calculated, the particle size of the manganese oxide was then calculated. The Fourier method was also used to calculate the mean square lattice strain of the manganese oxide and the results were as follows, where the particle size is equal to 7.9563 nm and the mean square strain equal to 0.3566 × 10 -4 . In order to determine the accuracy of the results of this method, other methods of analysis were used, such as the Debye - Scherrer method and Williamson–Hall method of analysis, and Modified Scherrer equation for calculating the particle size. The value of particle size and strain of these four methods was compared with the value of particle size and mean square strain of the Fourier method.
机译:在这项研究中,使用傅里叶分析法分析MnO(111),(200),(220),(311)和(222)的X射线衍射图。计算每个X射线线的粒径,然后计算锰氧化物的粒径。还使用傅里叶法计算了锰氧化物的均方晶格应变,结果如下:粒径等于7.9563 nm,均方应变等于0.3566×10 -4。为了确定该方法结果的准确性,使用了其他分析方法,例如Debye-Scherrer方法和Williamson-Hall分析方法,以及用于计算粒径的改良Scherrer方程。将这四种方法的粒径和应变值与傅里叶方法的粒径和均方应变值进行比较。

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