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Effect of Nitrogen Content on Hot Deformation Behavior and Grain Growth in Nuclear Grade 316LN Stainless Steel

机译:氮含量对核级316LN不锈钢热变形行为和晶粒长大的影响

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316LN stainless steel with 0.08%N (08N) and 0.17%N (17N) was compressed at 1073–1473 K and 0.001–10 s−1. The hot deformation behavior was investigated using stress-strain curve analysis, processing maps, and so forth. The microstructure was analyzed through electron backscatter diffraction analysis. Under most conditions, the deformation resistance of 17N was higher than that of 08N. This difference became more pronounced at lower temperatures. The strain rate sensitivity increased with increasing temperature for types of steel. In addition, the higher the N content, the higher the strain rate sensitivity. Hot deformation activation energy increased from 487 kJ/mol to 549 kJ/mol as N concentration was increased from 0.08% to 0.17%. The critical strain for initiation of dynamic recrystallization was lowered with increasing N content. In the processing maps, both power dissipation ratio and unstable region increased with increasing N concentration. In terms of microstructure evolution, N promoted dynamic recrystallization kinetic and decreased dynamic recrystallization grain size. The grain growth rate was lower in 17N than in 08N during heat treatment. Finally, it was found that N favored twin boundary formation.
机译:含0.08%N(08N)和0.17%N(17N)的316LN不锈钢在1073–1473 K和0.001-10 s-1下被压缩。使用应力-应变曲线分析,加工图等研究了热变形行为。通过电子背散射衍射分析来分析微观结构。在大多数情况下,17N的抗变形性高于08N。这种差异在较低温度下变得更加明显。对于钢种,应变率灵敏度随温度的升高而增加。另外,N含量越高,应变率灵敏度越高。随着N浓度从0.08%增加到0.17%,热变形活化能从487 kJ / mol增加到549 kJ / mol。随着N含量的增加,开始动态再结晶的临界应变降低。在处理图中,功率耗散率和不稳定区域都随着氮浓度的增加而增加。就微观组织演变而言,N促进了动态再结晶动力学并降低了动态再结晶晶粒尺寸。在热处理过程中,17N的晶粒生长速率低于08N的晶粒生长速率。最后,发现N有利于孪晶边界的形成。

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