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Effect of Nitrogen Content on Hot Deformation Behavior and Grain Growth in Nuclear Grade 316LN Stainless Steel

机译:氮含量对核级316LN不锈钢的热变形行为和晶粒生长的影响

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摘要

316LN stainless steel with 0.08%N (08N) and 0.17%N (17N) was compressed at 1073–1473 K and 0.001–10 s−1. The hot deformation behavior was investigated using stress-strain curve analysis, processing maps, and so forth. The microstructure was analyzed through electron backscatter diffraction analysis. Under most conditions, the deformation resistance of 17N was higher than that of 08N. This difference became more pronounced at lower temperatures. The strain rate sensitivity increased with increasing temperature for types of steel. In addition, the higher the N content, the higher the strain rate sensitivity. Hot deformation activation energy increased from 487 kJ/mol to 549 kJ/mol as N concentration was increased from 0.08% to 0.17%. The critical strain for initiation of dynamic recrystallization was lowered with increasing N content. In the processing maps, both power dissipation ratio and unstable region increased with increasing N concentration. In terms of microstructure evolution, N promoted dynamic recrystallization kinetic and decreased dynamic recrystallization grain size. The grain growth rate was lower in 17N than in 08N during heat treatment. Finally, it was found that N favored twin boundary formation.
机译:在1073-1473K和0.001-10S-1下压缩316LN具有0.08%N(08N)和0.17%N(17N)的不锈钢。使用应力 - 应变曲线分析,加工图等研究了热变形行为。通过电子反向散射衍射分析分析微观结构。在大多数条件下,17N的变形电阻高于08N。这种差异在较低温度下变得更加明显。随着钢的类型的温度升高,应变率灵敏度增加。另外,氮含量越高,应变率敏感性越高。由于N浓度从0.08%增加到0.08%至0.17%,热变形活性能量从487 kJ / mol增加到549 kJ / mol。随着N含量的增加,降低了用于引发动态再结晶的临界应变。在处理地图中,功率耗散比和不稳定区域随着N浓度的增加而增加。在微观结构演化方面,N促进动态再结晶动力学和降低的动态再结晶粒径。在热处理期间,晶粒生长速率比08N较低。最后,发现n有利于双边界形成。

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