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Effect of electron irradiation on gas sensing properties of Al-Zno

机译:电子辐照对Al-Zno气敏性能的影响

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Al–ZnO thin films are prepared by Silar method and are annealed at 450°C for 1?h. A selected number of samples are irradiated by high-energy electron beam and all are characterized by XRD, SEM and energy-dispersive X-ray spectroscopy. Both irradiated and non-irradiated samples are then placed independently inside a gas chamber kept at rotary vacuum. The gas chamber is maintained at a pressure of 0.20?mb and at a temperature of 350°C. Ethanol vapour is admitted in a controlled manner into the chamber and the resistance of the film is measured continuously before, during and after the admittance of the ethanol vapour. The experiment is repeated for different dosages of irradiation and different doping concentrations of Al and the resistance of the film getting reduced fast and considerably at the admittance of ethanol has been observed. The response and recovery time of the irradiated samples is compared with that of non-irradiated samples of the same doping concentration. It has been noted that both irradiated and non-irradiated samples show a response time of 1?s and recovery time of the irradiated samples is shorter than that of non-irradiated samples.
机译:Al-ZnO薄膜通过Silar方法制备,并在450°C退火1?h。选定数量的样品通过高能电子束辐照,并通过XRD,SEM和能量色散X射线光谱进行表征。然后将辐照的样品和未辐照的样品都分别放置在保持旋转真空的气室内。气室保持在0.20?mb的压力和350°C的温度。乙醇蒸气以受控的方式进入腔室,并且在乙醇蒸气的进入之前,期间和之后连续测量膜的电阻。对于不同的辐照剂量和不同的Al掺杂浓度重复进行该实验,并且观察到膜的电阻在乙醇的导纳下迅速而显着降低。将辐照样品的响应和恢复时间与相同掺杂浓度的未辐照样品的响应和恢复时间进行比较。已经注意到,被辐照和未辐照的样品都显示出1μs的响应时间,并且被辐照的样品的恢复时间短于未辐照的样品。

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