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Synthesis and characterization of ZnO nanostructures using palm olein as biotemplate

机译:以棕榈油精为模板,合成并表征ZnO纳米结构

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Background A green approach to synthesize nanomaterials using biotemplates has been subjected to intense research due to several advantages. Palm olein as a biotemplate offers the benefits of eco-friendliness, low-cost and scale-up for large scale production. Therefore, the effect of palm olein on morphology and surface properties of ZnO nanostructures were investigated. Results The results indicate that palm olein as a biotemplate can be used to modify the shape and size of ZnO particles synthesized by hydrothermal method. Different morphology including flake-, flower- and three dimensional star-like structures were obtained. FTIR study indicated the reaction between carboxyl group of palm olein and zinc species had taken place. Specific surface area enhanced while no considerable change were observed in optical properties. Conclusion Phase-pure ZnO particles were successfully synthesized using palm olein as soft biotemplating agent by hydrothermal method. The physico-chemical properties of the resulting ZnO particles can be tuned using the ratio of palm olein to Zn cation.
机译:背景技术由于具有许多优点,使用生物模板合成纳米材料的绿色方法已受到广泛研究。棕榈油精作为一种生物模板,具有生态友好,低成本和大规模生产的优势。因此,研究了棕榈油精对ZnO纳米结构的形貌和表面性能的影响。结果结果表明,棕榈油精作为生物模板可用于修饰水热法合成的ZnO颗粒的形状和尺寸。获得了包括片状,花状和三维星状结构在内的不同形态。 FTIR研究表明棕榈油精的羧基和锌物种之间已经发生了反应。比表面积增加,而光学性能未观察到显着变化。结论以棕榈油精为软生物模板剂,水热法成功合成了纯相ZnO颗粒。可以使用棕榈油精与Zn阳离子的比例来调节所得ZnO颗粒的物理化学性质。

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