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STRUCTURAL AND OPTICAL PROPERTIES OF ZnS NANOPARTICLES SYNTHESIZED BY MICROWAVE IRRADIATION METHOD

机译:微波辐射法合成ZnS纳米粒子的结构和光学性质

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ZnS nanoparticles were synthesized by Microwave assisted irradiation method. The obtained ZnS nanoparticles were characterized by XRD, SEM and UV-Vis spectroscopy. XRD characterization of the samples were taken which verify the crystalline form of the samples and also the average size of the nanocrystallites were measured by Debye- Scherrer formula as per the XRD spectrum, which was found to be around 6 nm. The surface morphology of the ZnS nanocrystallites was taken by Scanning Electron Microscopy. The UV-Visible absorption spectra of the nanocrystallites were taken and the optical bandgap of the ZnS nanocrystals were found to be 3.76 eV.
机译:微波辅助辐射法合成了ZnS纳米粒子。通过XRD,SEM和UV-Vis光谱对所得的ZnS纳米颗粒进行表征。进行样品的XRD表征,以验证样品的晶体形式,并根据XRD光谱,通过Debye-Scherrer公式测量纳米微晶的平均尺寸,发现其约为6 nm。 ZnS纳米晶体的表面形态通过扫描电子显微镜法获得。拍摄纳米晶体的紫外可见吸收光谱,发现ZnS纳米晶体的光学带隙为3.76eV。

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