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Residual monomer in a composite resin after light-curing with different sources, light intensities and spectra of radiation

机译:不同来源,光强度和辐射光谱光固化后复合树脂中的残留单体

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The purpose of this study was to investigate the amount of residual monomer in a composite resin after light-curing with different sources, light intensities and spectra of radiation. The resin specimens (4 mm in diameter; 2 mm thick) (n=5) were inserted in Plexglass matrixes and light-cured with a halogen lamp, LED and PAC units for 40, 40 and 5 s, respectively. The polymerized specimens were ground and 25 mg of each specimen were immersed in 8 mL 96% ethanol for 24 h to extract the residual monomer. The amount of residual monomer was determined by the standard straight line method. The light spectrum of the different LCUs was shot and processed through researches of the absorbation of the standard solutions at a level of lambda= 275 nm and their extracts. Data were analyzed statistically by variational dispersion analysis and Tukey-Kramer test at 5% significance level. It was observed that, the halogen lamp produced the smallest amount of monomer under sufficient light intensity. The spectrum of light radiation of PAC was within the limits of 450- 490 nm and was of extremely high intensity. This imposes the use of short-limited light impulses, but also might lead to deterioration quality of polymerization. The LED unit had the best spectral radiation. An increase of light intensity was proved necessary.
机译:这项研究的目的是研究在使用不同光源,光强度和辐射光谱进行光固化之后,复合树脂中残留的单体数量。将树脂样品(直径4毫米;厚度2毫米)(n = 5)插入Plexglass基质中,并分别用卤素灯,LED和PAC单元分别光固化40、40和5 s。研磨聚合的样品,将25 mg的每个样品浸入8 mL 96%乙醇中24 h,以提取残留的单体。残余单体的量通过标准直线法确定。通过研究λ= 275 nm的标准溶液及其提取物的吸收来拍摄和处理不同LCU的光谱。数据通过变化分散分析和Tukey-Kramer检验以5%的显着性水平进行统计分析。观察到,在足够的光强度下,卤素灯产生最小量的单体。 PAC的光辐射光谱在450-490nm的范围内,并且具有极高的强度。这强加了短时光脉冲的使用,但也可能导致聚合质量下降。 LED单元具有最佳的光谱辐射。证明增加光强度是必要的。

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