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Arsenic removal from synthetic waste water by CuO nano-flakes synthesized by aqueous precipitation method

机译:水沉淀法合成CuO纳米片去除合成废水中的砷

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摘要

Arsenic contamination in the drinking water is a serious issue affecting health of inhabitants of developing countries like India and Bangladesh and needs cost effective solutions. The nanomaterials having large surface area per unit volume could be useful adsorbent for water arsenic decontamination. The CuO nanomaterial synthesized by aqueous precipitation method. The obtained nanomaterial suspension sonicated for 15 min before centrifugation at 5,000 g for 10 min. Thoroughly washed and overnight dried pellets at 60 degrees C characterized by scanning electron microscope revealed nanoflakes structure of the pellets. The copper nanoflakes (CONF) have monoclinic CuO structure in XRD analysis. The kinetics of arsenic adsorption determined by varying arsenic content and dose of adsorbent for a period of 1 h revealed second order adsorption kinetics. The synthesized nano-flakes have potential application for arsenic removal from water well below safe limit.
机译:饮用水中的砷污染是一个严重的问题,影响到印度和孟加拉国等发展中国家居民的健康,因此需要经济有效的解决方案。每单位体积具有大表面积的纳米材料可以用作水砷净化的吸附剂。水沉淀法合成CuO纳米材料。将获得的纳米材料悬浮液超声处理15分钟,然后以5,000 g离心10分钟。通过扫描电子显微镜表征的在60℃下彻底洗涤并干燥过夜的粒料显示出粒料的纳米薄片结构。铜纳米薄片(CONF)在XRD分析中具有单斜晶CuO结构。通过改变砷含量和吸附剂剂量1 h来确定的砷吸附动力学揭示了二级吸附动力学。合成的纳米薄片具有潜在的应用,可用于从水中去除砷,其安全浓度远低于安全限值。

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