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Shear bond strengths between different zirconia cores and veneering ceramics and their susceptibility to thermocycling

机译:氧化锆芯和饰面陶瓷之间的剪切粘结强度及其对热循环的敏感性

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Objectives. The purpose of this study was to evaluate the shear bond strength between various commercial zirconia core and veneering ceramics, and to investigate the effect of thermocycling. Methods. The Schmitz-Schulmeyer test method was used to evaluate the core-veneer shear bond strength (SBS) of three zirconia core ceramics (Cercon Base, Vita In-Ceram YZ Cubes, DC-Zirkon) and their manufacturer recommended veneering ceramics (Cercon Ceram S, Vita VM9, IPS e.max Ceram). A metal ceramic system (Degudent U94, Vita VM13) was used as a control group for the three all-ceramic test groups (n = 30 specimens/group). Half of each group (n = 15) was thermocycled (5-55 ℃, 20,000 cycles). Subsequently, all specimens were subjected to shear force in a universal testing machine. Fractured specimens were evaluated microscopically to determine the failure mode. Results. The initial mean SBS values in MPa ± S.D. were 12.5 ± 3.2 for Vita In-Ceram YZ Cubes/Vita VM9, 11.5 ± 3.4 for DC-Zirkon/IPS e.max Ceram, and 9.4 ± 3.2 for Cercon Base/Cercon Ceram S. After thermocycling mean SBS values of 11.5 ± 1.7 MPa for DC-Zirkon/IPS e.max Ceram, 9.7 ± 4.2 MPa for Vita In-Ceram YZ Cubes/Vita VM9, and 9.6 ± 4.2 MPa for Cercon Base/Cercon Ceram S were observed. Neither the differences between the SBS values of the all-ceramic test groups nor the influence of thermocycling on all groups were statistically significant. Irrespective of thermocycling the metal ceramic control group (27.6 ± 12.1 MPa, 26.4 ± 13.4 MPa) exhibited significantly higher mean SBS than all three all-ceramic groups tested. The all-ceramic groups showed combined failure modes as cohesive in the veneering ceramic and adhesive at the interface, whereas the metal ceramic group showed predominately cohesive fractures. Significance. The results indicated that the SBS between zirconia core and veneering ceramics was not affected by thermocycling. None of the zirconia core and veneering ceramics could attain the high bond strength values of the metal ceramic combination.
机译:目标。这项研究的目的是评估各种商业氧化锆芯和饰面陶瓷之间的剪切粘结强度,并研究热循环的影响。方法。 Schmitz-Schulmeyer测试方法用于评估三种氧化锆芯陶瓷(Cercon Base,Vita In-Ceram YZ Cubes,DC-Zirkon)及其制造商推荐的贴面陶瓷(Cercon Ceram S)的芯-背板剪切粘结强度(SBS)。 ,Vita VM9,IPS e.max Ceram)。将金属陶瓷系统(Degudent U94,Vita VM13)用作三个全陶瓷测试组(n = 30个样本/组)的对照组。每组一半(n = 15)进行热循环(5-55℃,20,000个循环)。随后,所有样品在万能试验机中经受剪切力。显微镜下评估断裂的样品,以确定破坏模式。结果。初始平均SBS值MPa±S.D. Vita In-Ceram YZ多维数据集/ Vita VM9为12.5±3.2,DC-Zirkon / IPS e.max Ceram为11.5±3.4,Cercon Base / Cercon Ceram S为9.4±3.2。热循环后的平均SBS值为11.5±1.7观察到DC-Zirkon / IPS e.max Ceram的MPa,Vita In-Ceram YZ Cubes / Vita VM9的9.7±4.2 MPa和Cercon Base / Cercon Ceram S的9.6±4.2 MPa。所有陶瓷测试组的SBS值之间的差异或热循环对所有组的影响均无统计学意义。不论进行热循环,金属陶瓷对照组(27.6±12.1 MPa,26.4±13.4 MPa)均显示出比所有三个全陶瓷组均更高的平均SBS值。全陶瓷组表现出组合的破坏模式,如在饰面陶瓷和界面处的粘合剂内聚,而金属陶瓷组则主要表现出内聚破裂。意义。结果表明,氧化锆芯和饰面陶瓷之间的SBS不受热循环的影响。氧化锆芯和饰面陶瓷都无法达到金属陶瓷组合的高粘结强度值。

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