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Investigating the interaction mechanism and effect of different calcium sulfate whiskers on performance of asphalt binder

机译:研究不同硫酸钙晶须的相互作用机理及对沥青结合料性能的影响

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摘要

Three kinds of calcium sulfate whisker (CSW) and two types of asphalt binders were used to prepare the modification asphalt by mechanical stirring. The influence of the types and contents of CSW on the high temperature performance, deformation resistance property, temperature susceptibility performance, viscosity-temperature characteristic, rheological property and low temperature performance of asphalt binder were respectively analyzed by softening point test, ductility test, cone penetration test, Brookfield rotational viscosity test, dynamic shear rheometer (DSR) and bending beam rheometer (BBR). In addition, the interaction mechanism of CSW with asphalt binder was investigated by the Attenuated total reflection-Fourier transform infrared spectroscopy (ATR-FTIR), X-ray diffraction (XRD) analyzer and Scanning electron microscope (SEM). The results indicate that three CSWs can significantly improve the high temperature performance, rheological property and deformation resistance property of two asphalt binders, but will weaken their temperature susceptibility performance, viscosity-temperature characteristic and low temperature performance to some extent when CSWs contents range from 7 wt% to 11 wt%. The effect of CSWs on the performances of asphalt binder is related to the types of CSW and the kinds of base asphalt, respectively. The results of ATR-FTIR, XRD and SEM tests indicate that the interaction between CSWs and asphalt binder is physical adsorption and interleaving process. (C) 2019 Elsevier Ltd. All rights reserved.
机译:采用三种硫酸钙晶须(CSW)和两种沥青粘结剂通过机械搅拌制备改性沥青。通过软化点试验,延性试验,锥孔渗透试验,分别分析了CSW的种类和含量对沥青粘合剂的高温性能,抗变形性能,温度敏感性性能,黏温特性,流变性能和低温性能的影响。测试,布鲁克菲尔德旋转粘度测试,动态剪切流变仪(DSR)和弯曲梁流变仪(BBR)。此外,通过衰减全反射-傅里叶变换红外光谱(ATR-FTIR),X射线衍射(XRD)分析仪和扫描电子显微镜(SEM)研究了CSW与沥青粘合剂的相互作用机理。结果表明,三种CSWs可显着改善两种沥青胶结料的高温性能,流变性能和抗变形性能,但当CSWs含量在7以下时,会在一定程度上削弱其温度敏感性,粘度-温度特性和低温性能。 wt%至11wt%。 CSWs对沥青粘合剂性能的影响分别与CSW的类型和基础沥青的种类有关。 ATR-FTIR,XRD和SEM测试结果表明,CSW与沥青结合料之间的相互作用是物理吸附和交错过程。 (C)2019 Elsevier Ltd.保留所有权利。

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