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Microstructures and mechanical properties of Cu/Ti_3SiC_2/C/graphene nanocomposites prepared by vacuum hot-pressing sintering and hot isostatic pressing

机译:真空热压烧结和热等静压法制备的Cu / Ti_3SiC_2 / C /石墨烯纳米复合材料的组织和力学性能

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摘要

Copper-graphite composite is an ideal friction material due to its good heat resistance, wear resistance and friction coefficient stability. The addition of Ti3SiC2 can improve strength, hardness and wear resistance of copper-graphite alloy material without affecting its self-lubricating properties and electrical conductivity. Two dimensional graphene has become an attractive composite reinforcement owing to their unique electrical, mechanical and thermal properties. Cu/Ti3SiC2/C/Graphene naocomposite materials reinforced with graphene have been fabricated by vacuum hot-pressing sintering and hot isostatic pressing. Microstructures and mechanical properties of Cu/Ti3SiC2/C/Graphene naocomposite materials with different graphene contents have been systematically investigated. Microstructures of the composites were examined by optical microscopy, X-ray diffraction, back scattered electron imaging, scanning electron microscope with energy dispersive spectrometer and transmission electron microscope. The mechanical properties were determined from Brinell hardness, tensile, compressive and shear tests. Results demonstrated that there was an optimum value of graphene content which has an impact on microstructures and mechanical properties of Cu/Ti3SiC2/C/Graphene naocomposite materials. Based on graphene content on microstructure and mechanical properties of Cu/Ti3SiC2/C/Graphene naocomposite materials, strengthening and fracture mechanisms by graphene reinforcement have been analyzed.
机译:铜-石墨复合材料具有良好的耐热性,耐磨性和摩擦系数稳定性,是理想的摩擦材料。 Ti 3 SiC 2的添加可以改善铜石墨合金材料的强度,硬度和耐磨性,而不会影响其自润滑性能和导电性。二维石墨烯由于其独特的电,机械和热性能而成为有吸引力的复合增强材料。通过真空热压烧结和热等静压法制备了石墨烯增强的Cu / Ti3SiC2 / C /石墨烯复合材料。研究了不同石墨烯含量的Cu / Ti3SiC2 / C /石墨烯复合材料的微观结构和力学性能。通过光学显微镜,X射线衍射,反向散射电子成像,具有能谱仪的扫描电子显微镜和透射电子显微镜对复合材料的微观结构进行了检查。机械性能由布氏硬度,拉伸,压缩和剪切测试确定。结果表明,存在最佳的石墨烯含量值,这对Cu / Ti3SiC2 / C /石墨烯复合材料的微观结构和力学性能有影响。基于石墨烯含量对Cu / Ti3SiC2 / C /石墨烯复合材料的微观结构和力学性能的影响,分析了石墨烯增强的强化和断裂机理。

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