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Metal-free cascade radical cyclization of 1,6-enynes with aldehydes

机译：1,6-烯炔与醛的无金属级联自由基环化

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摘要

A new and efficient metal-free cascade cyclization of 1,6-enynes with aldehydes is developed for the synthesis of tricyclic fluorene derivatives. The reaction involves a radical process and one C(sp2)-C(sp~2) and two C(sp~2)-C(sp~3) bonds are formed simultaneously in one pot by using PivOH and TBHP.
机译：为合成三环芴衍生物，开发了一种新的，高效的无醛与醛的1,6-烯炔的无金属级联环化反应。该反应涉及自由基过程，并且通过使用PivOH和TBHP在一个罐中同时形成一个C（sp2）-C（sp-2）和两个C（sp-2）-C（sp-3）键。

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  • 来源
    《Chemical Communications》 |2014年第13期|1564-1566|共3页
  • 作者

    Jian-Yi Luo; Hui-Liang Hua; Zi-Sheng Chen; Zhao-Zhao Zhou; Yan-Fang Yang; Ping-Xin Zhou; Yu-Tao He; Xue-Yuan Liu; Yong-Min Liang;

  • 作者单位

    State Key Laboratory of Applied Organic Chemistry, Lanzhou University, and State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Science, Lanzhou 730000, P.R. China;

    State Key Laboratory of Applied Organic Chemistry, Lanzhou University, and State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Science, Lanzhou 730000, P.R. China;

    Department of Chemistry and Chemical Engineering, College of Science, Northwest A&F University, Yangling 712100, Shaanxi, China;

    State Key Laboratory of Applied Organic Chemistry, Lanzhou University, and State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Science, Lanzhou 730000, P.R. China;

    State Key Laboratory of Applied Organic Chemistry, Lanzhou University, and State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Science, Lanzhou 730000, P.R. China;

    State Key Laboratory of Applied Organic Chemistry, Lanzhou University, and State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Science, Lanzhou 730000, P.R. China;

    State Key Laboratory of Applied Organic Chemistry, Lanzhou University, and State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Science, Lanzhou 730000, P.R. China;

    State Key Laboratory of Applied Organic Chemistry, Lanzhou University, and State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Science, Lanzhou 730000, P.R. China;

    State Key Laboratory of Applied Organic Chemistry, Lanzhou University, and State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Science, Lanzhou 730000, P.R. China;

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  • 入库时间 2022-08-17 13:15:03

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