Novel Pd(Ⅱ)-catalysed N,O-bicyclisation as an efficient route to the 6-oxa-2-azabicyclo[3.2.1]octane skeleton

Peter Szolcsanyi; Tibor Gracza

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Novel Pd(Ⅱ)-catalysed N,O-bicyclisation as an efficient route to the 6-oxa-2-azabicyclo[3.2.1]octane skeleton

机译：新型Pd（Ⅱ）催化的N，O-双环化是通向6-氧杂-2-氮杂双环[3.2.1]辛烷骨架的有效途径

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1-(Benzyloxycarbonylamino)-hex-5-en-3-ol (5) undergoes a novel Pd(Ⅱ)/CuCl_2-catalysed bicyclisation to furnish the corresponding 6-oxa-2-azabicyclo[3.2.1]octane (6) in good yield.

机译：1-（苄氧羰基氨基）-己-5-烯-3-醇（5）经历新型Pd（Ⅱ）/ CuCl_2催化的双环化反应，以提供相应的6-氧杂-2-氮杂双环[3.2.1]辛烷（6）产量高。

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《Chemical Communications》 |2005年第31期|p.3948-3950|共3页
作者
Peter Szolcsanyi; Tibor Gracza;
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Department of Organic Chemistry, Slovak University of Technology, Radlinskeho 9, 812 37, Bratislava, Slovakia;

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正文语种 eng
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专利

1. Towards a general diastereoselective route to oxabicyclo[3.2.1]octanes via a gold-catalysed cascade reaction [J] . Fu Junkai, Gu Yueqing, Yuan Hao, Nature Communications . 2015,第Octa期

机译：通过金催化的级联反应向氧杂双环[3.2.1]辛烷的一般非对映选择性路线
2. Towards a general diastereoselective route to oxabicyclo[3.2.1]octanes via a gold-catalysed cascade reaction [J] . Junkai Fu, Yueqing Gu, Hao Yuan, Nature Communications . 2015,第1期

机译：通过金催化的级联反应向氧杂双环[3.2.1]辛烷的一般非对映选择性路线
3. The first diastereoselective synthesis of cinerins A-C, PAF-antagonistic macrophyllin-type bicyclo[3.2.1]octane neolignans, using a novel Pd-catalysed oxyarylation [J] . Ericsson D. Coy B., Luis E. Cuca S., Michael Sefkow Organic & biomolecular chemistry . 2010,第9期

机译：首次非对映选择性合成cinerins A-C，PAF拮抗大叶绿素型双环[3.2.1]辛烷新木脂素，使用新型Pd催化的酰氧基化反应
4. Vibrational-circular-dichroism spectra of five methyl-substituted 68-dioxabicyclo3.2.1octanes [C] . Thomas Eggimann, Hal Wieser International conference on Fourier transform spectroscopy . 1992

机译：五个甲基取代的68-二恶英的二色性光谱3.2.1辛烷值
5. I. BRIDGED TRANS-CYCLOHEPTENES: BICYCLO(3.2.2)NON-1-ENE, BICYCLO(3.2.2)NON-1(7)-ENE, BICYCLO(3.2.1)OCT-1-ENE, AND BICYCLO(3.2.1)OCT-1(7)-ENE. II. NEOPENYL REARRANGEMENTS: THE INTERCONVERSIONS OF BICYCLO(3.2.2)NON-1-YL, BICYCLO(3.2.1)-OCTANE-1-METHYL, AND BICYCLO(2.2.2)OCTANE-1-METHYL SYSTEMS. [D] . CHONG, JOSHUA ANTHONY. 1971

机译：I.桥接跨环蛋白：双环（3.2.2）NON-1-ENE，双环（3.2.2）NON-1（7）-ENE，双环（3.2.1）OCT-1-ENE和双环（3.2） .1）OCT-1（7）-ENE。二。新戊基重排：Bicyclo（3.2.2）NON-1-YL，BICYCLO（3.2.1）-OCTANE-1-甲基和BICYCLO（2.2.2）OCTANE-1-甲基系统的互换。
6. Towards a general diastereoselective route to oxabicyclo3.2.1octanes via a gold-catalysed cascade reaction [O] . Junkai Fu, Yueqing Gu, Hao Yuan, -1

机译：通过金催化的级联反应向氧杂双环3.2.1辛烷的一般非对映选择性路线
7. An Efficient Route to All Stereoisomeric Enantiopure 6-Amino-3-alkyl-3-azabicyclo3.2.1octane-6-carboxylic Acids [O] . -1

机译：与所有立体异构体对映射6-氨基-3-烷基-3-氮杂环三甲基 - 6-羧酸的有效途径3.2.1

Novel Pd(Ⅱ)-catalysed N,O-bicyclisation as an efficient route to the 6-oxa-2-azabicyclo[3.2.1]octane skeleton

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