Simple synthesis of 3-Acyl-5-Alkyl(aryl)isoxazoles from terminal alkynes and nitrates of alkaline metals or ammonium

Rogachev Victor O.; Filimonov Victor D.; Kulmanakova Julya Y.u.; Yusubov Mehman S.; Bender Wolfgang

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Simple synthesis of 3-Acyl-5-Alkyl(aryl)isoxazoles from terminal alkynes and nitrates of alkaline metals or ammonium

机译：从末端炔烃和碱金属或铵的硝酸盐简单合成3-酰基5-烷基（芳基）异恶唑

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摘要

A simple and general synthesis of 3-acyl-5-alkyl(aryl)isoxazoles by reaction of terminal alkynes with nitrates in acetic acid in the presence of SO₃ or alkaline salts is described.

机译：描述了在SO 3或碱金属盐存在下，末端炔烃与硝酸盐在乙酸中反应的一种3-酰基-5-烷基（芳基）异恶唑的简单通用合成方法。

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《Central European Journal of Chemistry》 |2005年第3期|p.370-376|共7页
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Rogachev Victor O.; Filimonov Victor D.; Kulmanakova Julya Y.u.; Yusubov Mehman S.; Bender Wolfgang;
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1. Simple synthesis of 3-Acyl-5-Alkyl(aryl)isoxazoles from terminal alkynes and nitrates of alkaline metals or ammonium [J] . Victor O.Rogachev, Victor D.Filimonov, Julya Yu.Kulmanakova Central European Journal of Chemistry . 2005,第3期

机译：从末端炔烃和碱金属或铵的硝酸盐简单合成3-酰基5-烷基（芳基）异恶唑
2. tert-Butyl Nitrite-Mediated Domino Synthesis of Isoxazolines and Isoxazoles from Terminal Aryl Alkenes and Alkynes [J] . Sau Prasenjit, Santra Sourav Kumar, Rakshit Amitava, The Journal of Organic Chemistry . 2017,第12期

机译：亚硝酸盐介导的异恶唑啉和异恶唑末端甲基烯烃和炔醇的叔丁酯
3. A sequential synthesis of substituted furans from aryl alkynes and ketones involving a cerium(IV) ammonium nitrate (CAN)-mediated oxidative cyclization [J] . Sridhar Undeela, Joshi P. Ramchandra, Rajeev S. Menon Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2014,第41期

机译：从芳基炔烃和酮顺序合成取代呋喃，涉及硝酸铈（IV）铵（CAN）介导的氧化环化
4. Effects of Ammonium to Nitrate Ratios on Substrate pH Shifts duringGrowth of Calibrachoa with Alkaline Water [C] . Matthew D. Taylor, Dieter Lohr Annual Meeting of the International^Plant^Propagators ^Society . 2013

机译：碱性水分碱对碱pH转移酸血管生长碱的影响
5. Development of Group 4 Metallocene/Palladium Bimetallic-Catalyzed Reductive Cross-Coupling Reaction between Alkynes and Aryl Halides [D] . 髙橋　慶多 2019

机译：炔烃与芳基卤化物之间第4族茂金属/钯双金属催化的还原交叉偶联反应的研究
6. Selective oxymetalation of terminal alkynes via 6-endo cyclization: mechanistic investigation and application to the efficient synthesis of 4-substituted isocoumarins [O] . Yuji Kita, Tetsuji Yata, Yoshihiro Nishimoto, 2018

机译：通过6-内基环化对末端炔烃的选择性氧化金属化：机理研究及其在4-取代异香豆素有效合成中的应用
7. tert-Butyl Nitrite-Mediated Domino Synthesis of Isoxazolines and Isoxazoles from Terminal Aryl Alkenes and Alkynes [O] . -1

机译：亚硝酸盐介导的异恶唑啉和异恶唑末端甲基烯烃和炔醇的叔丁酯

Simple synthesis of 3-Acyl-5-Alkyl(aryl)isoxazoles from terminal alkynes and nitrates of alkaline metals or ammonium

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