High intensity x-ray diffraction in transmission mode employing an analog of Poisson's spot

摘要

Poisson's spot is a diffraction phenomenon producing an intensity maximum at the center of the geometric shadow of circular opaque objects. In an analog of the Poisson spot experiment, we show that a tubular cone of x-rays incident upon a crystalline sample produces diffraction spots or foci, corresponding to Bragg maxima within a transmission shadow. We discuss the beam geometry and the intensity gain recorded at the foci in transmission mode. We describe the geometric growth and decay of the foci over a linear axis with the aid of a movie sequence synchronized with the plotting of a diffractogram. The mean signal of a small central area in each successive camera image provides the intensity data for the diffractogram.