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Green synthesis and characterization of gelatin-based and sugar-reduced silver nanoparticles

机译:明胶和减糖的银纳米粒子的绿色合成和表征

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摘要

Silver nanoparticles (Ag-NPs) have been successfully prepared with simple and “green” synthesis method by reducing Ag+ ions in aqueous gelatin media with and in the absence of glucose as a reducing agent. In this study, gelatin was used for the first time as a reducing and stabilizing agent. The effect of temperature on particle size of Ag-NPs was also studied. It was found that with increasing temperature the size of nanoparticles is decreased. It was found that the particle size of Ag-NPs obtained in gelatin solutions is smaller than in gelatin–glucose solutions, which can be related to the rate of reduction reaction. X-ray diffraction, ultraviolet-visible spectra, transmission electron microscopy, and atomic force microscopy revealed the formation of monodispersed Ag-NPs with a narrow particle size distribution.
机译:银纳米颗粒(Ag-NPs)已通过简单且“绿色”的合成方法成功制备,该方法通过在有或没有葡萄糖作为还原剂的情况下,在水性明胶介质中还原Ag + 离子。在这项研究中,明胶首次用作还原剂和稳定剂。还研究了温度对Ag-NPs粒径的影响。已经发现,随着温度升高,纳米颗粒的尺寸减小。发现明胶溶液中获得的Ag-NPs的粒径小于明胶-葡萄糖溶液中的粒径,这可能与还原反应的速率有关。 X射线衍射,紫外可见光谱,透射电子显微镜和原子力显微镜揭示了单分散的Ag-NP的形成,其粒径分布较窄。

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