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Study on Micro Interfacial Charge Motion of Polyethylene Nanocomposite Based on Electrostatic Force Microscope

机译:基于静电力显微镜的聚乙烯纳米复合材料微界面电荷运动研究

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摘要

The interface area of nano-dielectric is generally considered to play an important role in improving dielectric properties, especially in suppressing space charge. In order to study the role of interface area on a microscopic scale, the natural charge and injected charge movement and diffusion on the surface of pure LDPE and SiO /LDPE nanocomposite were observed and studied by gradual discharge under electrostatic force microscope (EFM). It was detected that the charge in SiO /LDPE nanocomposite moved towards the interface area and was captured, which indicates that the charge was trapped in the interface area and formed a barrier to the further injection of charge and improving the dielectric performance as a result. Moreover, pulsed electro-acoustic (PEA) short-circuited test after charge injection was carried out, and the change of total charge was calculated. The trend of charge decay in the EFM test is also generally consistent with that in PEA short-circuit test and can be used to verify one another. The results revealed the law of charge movement and verified the interface area can inhibit space charge injection in nano-dielectric at the microscale, which provides an experimental reference for relevant theoretical research.
机译:通常认为纳米介电体的界面面积在改善介电性能,特别是抑制空间电荷方面起重要作用。为了在微观尺度上研究界面区域的作用,在静电力显微镜(EFM)下通过逐步放电观察和研究了纯LDPE和SiO / LDPE纳米复合材料表面的自然电荷和注入电荷的运动和扩散。检测到SiO / LDPE纳米复合材料中的电荷向界面区域移动并被捕获,这表明电荷被捕获在界面区域中,并形成了进一步注入电荷并改善介电性能的屏障。另外,进行电荷注入后的脉冲电声(PEA)短路试验,算出总电荷的变化。 EFM测试中的电荷衰减趋势通常也与PEA短路测试中的电荷衰减趋势一致,并且可以相互验证。结果揭示了电荷运动的规律,并验证了界面区域可以在微观尺度上抑制纳米电介质中的空间电荷注入,为相关的理论研究提供了实验参考。

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