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Speed sintering translucent zirconia for chairside one-visit dental restorations: Optical mechanical and wear characteristics

机译:高速烧结半透明氧化锆用于椅子旁一遍牙科修复:光学机械和磨损特性

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摘要

The fabrication of zirconia dental restorations is a time-consuming process due to traditional slow sintering schemes; zirconia (Y-TZP) produced by these conventional routes are predominantly opaque. Novel speed sintering protocols have been developed to meet the demand for time and cost effective chairside CAD/CAM-produced restorations, as well as to control ceramic microstructures for better translucency. Although the speed sintering protocols have already been used to densify dental Y-TZP, the wear properties of these restorations remain elusive. Fast heating and cooling rates, as well as shorter sintering dwell times are known to affect the microstructure and properties of zirconia. Thus, we hypothesize that speed sintered zirconia dental restorations possess distinct wear and physical characteristics relative to their conventionally sintered counterparts. Glazed monolithic molar crowns of translucent Y-TZP (inCoris TZI, Sirona) were fabricated using three distinct sintering profiles: Super-speed (>SS, 1580 °C, dwell time 10 min), Speed (>S, 1510 °C, dwell time 25 min), and Long-term (>LT, 1510 °C, dwell time 120 min). Microstructural, optical and wear properties were investigated. Crowns that were super-speed sintered possessed higher translucency. Areas of mild and severe wear were observed on the zirconia surface in all groups. Micropits in the wear crater were less frequent for the LT group. Groups >S and >SS exhibited more surface pits, which caused a scratched steatite surface that is associated with a greater volume loss. Tetragonal to monoclinic phase transformation, resulting from the sliding wear process, was present in all three groups. Although all test groups had withstood thermo-mechanical challenges, the presence of hairline cracks emanating from the occlusal wear facets and extending deep into the restoration indicates their susceptibility to fatigue sliding contact fracture.
机译:由于传统的慢速烧结方案,氧化锆牙修复体的制造是一个耗时的过程。这些常规路线产生的氧化锆(Y-TZP)主要是不透明的。已经开发出新颖的速度烧结方案,以满足对时间和成本效益高的椅子旁CAD / CAM生产的修复体的需求,并控制陶瓷微结构以获得更好的半透明性。尽管已经使用速度烧结方案来致密化牙科Y-TZP,但这些修复体的磨损性能仍然难以捉摸。已知快速的加热和冷却速率以及较短的烧结停留时间会影响氧化锆的微观结构和性能。因此,我们假设快速烧结的氧化锆牙科修复物相对于其传统的烧结副本具有明显的磨损和物理特性。使用三种不同的烧结轮廓制造了半透明Y-TZP(在Sirona的Coris TZI)上釉的整体式磨牙冠:超高速(> SS ,1580°C,停留时间10分钟),速度( > S ,1510°C,停留时间25分钟)和长期(> LT ,1510°C,停留时间120分钟)。研究了显微组织,光学和磨损性能。超高速烧结的牙冠具有更高的半透明性。所有组的氧化锆表面均观察到轻度和重度磨损区域。对于LT组,磨损坑中的微坑频率较低。 > S 和> SS 组显示出更多的表面凹坑,这导致划痕的滑石表面与更大的体积损失相关。在所有三个组中都存在由滑动磨损过程引起的四方向单斜相转变。尽管所有测试组都经受住了热机械挑战,但从咬合磨损面发散并延伸到修复体深处的发际线裂纹的存在表明它们对疲劳滑动接触断裂的敏感性。

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