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Effect of nitrogen on grain growth and formability of Ti-stabilized ferritic stainless steels

机译:氮对钛稳定铁素体不锈钢晶粒长大和可成形性的影响

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摘要

The relationship between the grain size of as-cast and cold rolled 16%Cr ferritic stainless steel and the surface roughness defect, called ridging during forming was investigated. The ridging height corresponded to the grain size of the as-cast sample. The nitrogen content of 140 ppm yielded the minimum grain size and the minimum ridging height observed, whereas the nitrogen content of 50 ppm yielded the maximum grain size and the maximum ridging height observed. Ridging results from different plastic anisotropies of band structure composed of colonies. Through the EBSD analysis, the texture of mixed colonies composed of ND//{112} and ND//{331} in the 50 ppm nitrogen steel underwent more severe ridging than the randomly texture in the 140 ppm nitrogen steel sample. Therefore, an effective means to reduce the ridging of ferritic stainless steel during the forming process is to form a random texture by enhancing the formation of fine equiaxed grain during the casting process. During equal holding times at 1200 °C, the 80 ppm nitrogen sample was definitely coarsened, whereas the 200 ppm nitrogen sample underwent slower grain growth. Zener pinning force, which is proportional to the number of TiN particles on grain boundaries, was relatively strong in samples of 200 ppm nitrogen content, corresponding to slower grain growth. Although the Zener pinning force great affected with increasing nitrogen content, there may not affect the trend of initial cast grain size to be changed as much during annealing.
机译:研究了铸态和冷轧16%Cr铁素体不锈钢的晶粒尺寸与表面粗糙度缺陷之间的关系,这种缺陷被称为成形时的皱纹。皱纹高度对应于铸态样品的晶粒尺寸。氮含量为140 ppm时,可以观察到最小的晶粒度和最小皱纹高度;而氮含量为50 ppm时,可以观察到最大的晶粒度和皱纹高度。起皱起因于由菌落组成的能带结构的不同塑性各向异性。通过EBSD分析,与140 ppm氮钢样品中的随机织构相比,在50 ppm氮钢中由ND // {112}和ND // {331}组成的混合菌落的纹理更剧烈起皱。因此,在成形过程中减少铁素体不锈钢起皱的有效方法是通过在铸造过程中增强细等轴晶粒的形成来形成无规织构。在1200 C的相等保持时间下,80 ppm的氮样品确实被粗化,而200 ppm的氮样品的晶粒生长变慢。齐纳钉扎力与晶粒边界上的TiN颗粒数量成正比,在200 ppm氮含量的样品中相对较强,这意味着晶粒生长较慢。尽管齐纳钉扎力随氮含量的增加而受到很大的影响,但可能不会影响退火过程中初始铸造晶粒尺寸变化的趋势。

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