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Synthesis and characterization of dextran-coated iron oxide nanoparticles

机译:葡聚糖包覆的氧化铁纳米粒子的合成与表征

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摘要

Synthesis and characterization of iron oxide nanoparticles coated with a large molar weight dextran for environmental applications are reported. The first experiments involved the synthesis of iron oxide nanoparticles which were coated with dextran at different concentrations. The synthesis was performed by a co-precipitation technique, while the coating of iron oxide nanoparticles was carried out in solution. The obtained nanoparticles were characterized by using scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction spectrometry, Fourier transform infrared spectroscopy and superconducting quantum interference device magnetometry. The results demonstrated a successful coating of iron oxide nanoparticles with large molar weight dextran, of which agglomeration tendency depended on the amount of dextran in the coating solution. SEM and TEM observations have shown that the iron oxide nanoparticles are of about 7 nm in size.
机译:报道了用于环境应用的涂覆有大分子量右旋糖酐的氧化铁纳米颗粒的合成和表征。最初的实验涉及氧化铁纳米颗粒的合成,这些纳米颗粒被不同浓度的葡聚糖包被。通过共沉淀技术进行合成,同时在溶液中进行氧化铁纳米粒子的涂覆。通过扫描电子显微镜(SEM),透射电子显微镜(TEM),X射线衍射光谱,傅里叶变换红外光谱和超导量子干涉仪磁强分析对所得纳米颗粒进行表征。结果表明,用大分子量的右旋糖酐成功涂覆了氧化铁纳米颗粒,其团聚趋势取决于涂覆溶液中右旋糖酐的量。 SEM和TEM观察表明,氧化铁纳米粒子的尺寸约为7 nm。

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