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Synthesis and X-ray Crystal Structure of Meso-557121214-hexamethyl-14811-tetraazacyclotetradecane-18-di-(1-methyl-naphthalene)

机译：Meso-557121214-六甲基-14811-四氮杂环十四烷-18-二-（1-甲基萘）的合成及X射线晶体结构

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The pendant-arm macrocycle, meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene) has been synthesized and its single crystal structure determined. The molecule crystallizes in a primitive monoclinic cell, with the space group P21/a (#14). The cell dimensions are a = 10.778(3)Å, b = 13.809(3) Å, c = 11.420(2) Å, ∃ = 102.49(2)°, volume = 1659.5(6) Å³.

机译：已合成了侧链大环中观5,5,5,7,12,12,14-六甲基-1,4,8,11-四氮杂环十四烷-1,8-二-（1-甲基萘），并且其单晶结构确定。该分子在原始单斜细胞中结晶，空间群为P21 / a（＃14）。像元尺寸为a = 10.778（3）Å，b = 13.809（3）Å，c = 11.420（2）Å，∃= 102.49（2）°，体积= 1659.5（6）Å^{3 。}

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期刊名称 Molecules
作者
Robert I. Haines; Dean R. Hutchings;
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作者单位

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年(卷),期 2003(8),2
年度 2003
页码 243–250
总页数 8
原文格式 PDF
正文语种
中图分类分子生物学;
关键词
Pendant-arm macrocycle crystal structure 1-methylnaphthalene;

机译：悬臂大环;晶体结构;1-甲基萘;

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Synthesis and X-ray Crystal Structure of Meso-557121214-hexamethyl-14811-tetraazacyclotetradecane-18-di-(1-methyl-naphthalene)

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