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The Global Volatile Signature of Veal via Solid-phase Microextraction and Gas Chromatography-mass Spectrometry

机译:固相微萃取和气相色谱-质谱联用分析小牛肉的全球挥发性特征

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摘要

The volatile composition of veal has yet to be reported and is one of the important factors determining meat character and quality. To identify the most important aroma compounds in veal from Holstein bull calves fed one of three diets, samples were subjected to solid-phase microextraction (SPME) combined with gas chromatography-quadrupole mass spectrometry (GC-MS). Most of the important odorants were aldehydes and alcohols. For group A (veal calves fed entirely on milk for 90 d before slaughter), the most abundant compound class was the aldehydes (52.231%), while that was alcohols (26.260%) in group C (veal calves fed starter diet for at least 60 d before slaughter). In both classes the absolute percentages of the volatile compounds in veal were different indicating that the veal diet significantly (p<0.05) affected headspace volatile composition in veal as determined by principal component analysis (PCA). Twenty three volatile compounds showed significance by using a partial least-squared discriminate analysis (PLS-DA) (VIP>1). The establishment of the global volatile signature of veal may be a useful tool to define the beef diet that improves the organoleptic characteristics of the meat and consequently impacts both its taste and economic value.
机译:小牛肉的挥发性成分尚未被报道,并且是决定肉质和品质的重要因素之一。为了鉴定喂食三种日粮之一的荷斯坦公牛犊牛小牛肉中最重要的香气化合物,将样品进行固相微萃取(SPME)结合气相色谱-四极杆质谱(GC-MS)。大多数重要的增香剂是醛和醇。对于A组(屠宰前90天完全用牛犊喂养的小牛犊),最丰富的化合物类别是醛(52.231%),而C组(小牛饲喂初学者饮食的小牛犊)中的酒精含量最高(26.260%)。屠宰前60天)。在这两个类别中,小牛肉中挥发性化合物的绝对百分比均不同,这表明小牛肉日粮显着(p <0.05)影响了小牛肉中顶空挥发性成分(通过主成分分析(PCA)确定)。通过使用偏最小二乘判别分析(PLS-DA)(VIP> 1),发现了23种挥发性化合物。建立小牛肉的全球挥发性特征可能是定义牛肉饮食的有用工具,牛肉饮食可以改善肉的感官特性,从而影响其味道和经济价值。

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