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Hydrogen Embrittlement Behavior of 18Ni 300 Maraging Steel Produced by Selective Laser Melting

机译:选择性激光熔炼生产的18Ni 300马氏体时效钢的氢脆行为

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摘要

A study was performed to investigate the hydrogen embrittlement behavior of 18-Ni 300 maraging steel produced by selective laser melting and subjected to different heat treatment strategies. Hydrogen was pre-charged into the tensile samples by an electro-chemical method at the constant current density of 1 A m−2 and 50 A m−2 for 48 h at room temperature. Charged and uncharged specimens were subjected to tensile tests and the hydrogen concentration was eventually analysed using quadrupole mass spectroscopy. After tensile tests, uncharged maraging samples showed fracture surfaces with dimples. Conversely, in H-charged alloys, quasi-cleavage mode fractures occurred. A lower concentration of trapped hydrogen atoms and higher elongation at fracture were measured in the H-charged samples that were subjected to solution treatment prior to hydrogen charging, compared to the as-built counterparts. Isothermal aging treatment performed at 460 °C for 8 h before hydrogen charging increased the concentration of trapped hydrogen, giving rise to higher hydrogen embrittlement susceptibility.
机译:进行了一项研究,以研究通过选择性激光熔化并经受不同热处理策略的18-Ni 300马氏体时效钢的氢脆行为。在1 A m -2 和50 A m -2 的恒定电流密度下,通过电化学方法将氢预充入拉伸样品中48 h。室内温度。对带电和不带电的样品进行拉伸测试,最终使用四极杆质谱分析法分析氢浓度。拉伸测试后,未充电的马氏体样品显示出带有凹痕的断裂表面。相反,在含氢合金中,发生了准裂解模式的断裂。与建成时的样品相比,在充氢之前进行固溶处理的充氢样品中,捕获的氢原子浓度较低,断裂伸长率较高。在充氢之前,在460°C下进行了8h的等温时效处理,以增加捕集的氢的浓度,从而提高了氢脆化的敏感性。

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