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Reinforcement of PMMA Denture Base Material with a Mixture of ZrO2 Nanoparticles and Glass Fibers

机译:ZrO2纳米粒子和玻璃纤维的混合物增强PMMA假牙基体材料

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摘要

This study is aimed at evaluating the hybrid reinforcement effects of zirconium oxide nanoparticles (nano-ZrO2) and glass fibers (GFs) at different ratios on the flexural and impact strengths of a polymethylmethacrylate (PMMA) denture base. A total of 160 specimens were fabricated from heat-polymerized acrylic resins using the water bath technique. For the control group, the specimens did not receive any additions; for the test group, different concentrations of nano-ZrO2/GFs at 5% of the PMMA polymer were added. The concentrations of nano-ZrO2/GFs were as follows: 5%–0%, 4%–1%, 3%–2%, 2.5%–2.5%, 2%–3%, 1%–4%, and 0%–5%. The flexural strength was measured using the three-point bending test. The impact strength was measured using the Charpy impact test. Results were tabulated and analyzed using one-way analysis of variance (ANOVA) and the Tukey–Kramer multiple comparison test (p ≤ 0.05). The flexural and impact strengths of PMMA-nano-ZrO2 + GF composites were significantly improved when compared with those of pure PMMA (p < 0.05). The maximum flexural strength (94.05 ± 6.95 MPa) and impact strength (3.89 ± 0.46 kJ/m2) were obtained with PMMA (2.5%)ano-ZrO2 + 2.5% GF mixtures and could be used for removable prosthesis fabrication.
机译:这项研究旨在评估不同比例的氧化锆纳米颗粒(nano-ZrO2)和玻璃纤维(GFs)对聚甲基丙烯酸甲酯(PMMA)义齿基托的弯曲强度和冲击强度的混合增强作用。使用水浴技术由热聚合丙烯酸树脂制成总共160个样品。对于对照组,标本没有增加。对于测试组,在5%的PMMA聚合物中添加了不同浓度的纳米ZrO2 / GF。纳米ZrO2 / GFs的浓度如下:5%–0%,4%–1%,3%–2%,2.5%–2.5%,2%–3%,1%–4%和0 %–5%。使用三点弯曲试验测量弯曲强度。使用夏比冲击试验测量冲击强度。使用单向方差分析(ANOVA)和Tukey–Kramer多重比较检验(p≤0.05)将结果制成表格并进行分析。与纯PMMA相比,PMMA-纳米-ZrO2 + GGF复合材料的弯曲强度和冲击强度得到了显着提高(p <0.05)。使用2.5%PMMA /纳米ZrO2 + 2.5%GF混合物可获得最大抗弯强度(94.05±6.95 MPa)和冲击强度(3.89±0.46 kJ / m 2 ),可以使用用于可拆卸的假体制造。

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