Tetracarbonylbis(η5-cyclopentadienyl)bis[(dec-9-en-1-yl)diphenylphosphine]dimolybdenum(0)(Mo—Mo) tetrahydrofuran disolvate

机译：四羰基双（η5-环戊二烯基）双[（癸-9-烯-1-基）二苯基膦]二钼（0）（Mo-Mo）四氢呋喃二溶剂化物

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The asymmetric unit of the title compound, [Mo2(η⁵-C5H5)2(C22H29P)2(CO)4]·2C4H8O, contains two half-molecules of the organometallic species and two solvent molecules. Both organometallic molecules are completed by crystallographic inversion symmetry, yielding dimeric units with Mo—Mo single-bond lengths of 3.2703 (6) and 3.2548 (6) Å. Each Mo atom is also coordinated by an η⁵-cyclopentdienyl ligand, two carbonyl ligands, and a (dec-9-en-1-yl)diphenylphosphine ligand.

机译：标题化合物[Mo2（η^{5 -C5H5）2（C22H29P）2（CO）4]·2C4H8O的不对称单元包含两个有机金属半分子和两个溶剂分子。两种有机金属分子均通过晶体学反演对称性完成，生成具有Mo-Mo单键长度为3.2703（6）和3.2548（6）Å的二聚体单元。每个Mo原子也由η^{5 -环戊二烯基配体，两个羰基配体和（dec-9-en-1-yl）二苯基膦配体配位。}}

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期刊名称 Acta Crystallographica Section E: Crystallographic Communications
作者
Ginger Shultz; Lev N. Zakharov; David R Tyler;
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作者单位

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年(卷),期 2016(65),Pt 12
年度 2016
页码 m1545
总页数 20
原文格式 PDF
正文语种
中图分类生化遗传学;生化药理学;
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专利

1. Tetracarbonylbis(η5-cyclopentadienyl)bis(diphenylphosphine)dimolybdenum(Mo—Mo) hexane solvate [J] . Boss#233, S.A., Shultz G.V., Acta Crystallographica Section E: Crystallographic Communications . 2008,第7期

机译：Tetracarbonylbis(η5-cyclopentadienyl)bis(diphenylphosphine)dimolybdenum(Mo—Mo) hexane solvate
2. Crystal structures of fac-tri-carbonyl-chlorido-(6,6′-dihy-droxy-2,2′-bi-pyridine)-rhenium(I) tetra-hydro-furan monosolvate and fac-bromido-tricarbon-yl(6,6′-dihy-droxy-2,2′-bi-pyridine)-manganese(I) tetra-hydro-furan monosolvate [J] . Lense S., Piro N.A., Kassel S.W., Acta Crystallographica Section E: Crystallographic Communications . 2016,第8期

机译：fac-三羰基-氯-（6,6'-dihy-droxy-2,2'-联吡啶）-r（I）四氢呋喃单溶剂化物和fac-溴代三碳基（ 6,6'-dance-droxy-2,2'-bi-吡啶）-锰（I）四氢呋喃单溶剂化物
3. Crystal structures of fac-tri-carbonyl-chlorido-(6,6′-dihy-droxy-2,2′-bi-pyridine)-rhenium(I) tetra-hydro-furan monosolvate and fac-bromido-tricarbon-yl(6,6′-dihy-droxy-2,2′-bi-pyridine)-manganese(I) tetra-hydro-furan monosolvate [J] . Lense S., Piro N.A., Kassel S.W., Acta Crystallographica Section E: Crystallographic Communications . 2016,第8期

机译：fac-三羰基-氯-（6,6'-dihy-droxy-2,2'-联吡啶）-r（I）四氢呋喃单溶剂化物和fac-溴代三碳基（ 6,6'-dance-droxy-2,2'-bi-吡啶）-锰（I）四氢呋喃单溶剂化物
4. Influences of Humic Acids on the Pattern of Oxidation Products of Tetrabromobisphenol a Derived from a Catalytic System using Iron(III)- tetrakis(p-sulfophenyl)porphyrin and KHSO 5 [C] . Masami Fukushima, Yosuke Ishida, Satoko Shigematsu International Meeting of the International Humic Substances Society . 2010

机译：利用铁（III） - 四（对硫苯基）卟啉和KHSO 5，腐殖酸对催化体系衍生催化体系衍生催化体系的氧化产物图案的影响
5. The synthesis of bis(dimolybdenum)-1,3,5,7-tetrakis(2-pyridylimino) benzodipyrrole as a precursor for an inorganic, quadruple bond containing polymer. [D] . Kavanaugh, David John. 1993

机译：双（二钼）-1,3,5,7-四（2-吡啶基氨基）苯并二吡咯的合成，作为含有无机四键的聚合物的前体。
6. Tetracarbonylbis(η5-cyclopentadienyl)bis(diphenylphosphine)dimolybdenum(Mo—Mo) hexane solvate [O] . Ginger V. Shultz, Stephanie A. Bossé, Lev N. Zakharov, 2008

机译：四碳基双（η5-环戊二基）双（二苯基膦）二钼（Mo-Mo）己烷溶剂化物
7. Tetracarbonylbis(η5-cyclopentadienyl)bis[(dec-9-en-1-yl)diphenylphosphine]dimolybdenum(0)(Mo—Mo) tetrahydrofuran disolvate [O] . Shultz, Ginger, Zakharov, Lev N., Tyler, David R 2009

机译：四羰基双（η5-环戊二烯基）双[（癸-9-烯-1-基）二苯基膦]二钼（0）（Mo-Mo）四氢呋喃二溶剂化物
8. Reversible Addition of Carbon Monoxide to Tetracarbonyl bis(eta 5-pentamethylcyclopenta-dienyl)dimolybdenum. [R] . Ginley, D. S., Wrighton, M. S. 1975

机译：可逆地加成一氧化碳到四羰基双（η5-五甲基环戊二烯基）二钼。

Tetra­carbonyl­bis(η5-cyclo­penta­dienyl)bis[(dec-9-en-1-yl)diphenyl­phosphine]dimolybdenum(0)(Mo—Mo) tetra­hydro­furan disolvate

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Tetracarbonylbis(η5-cyclopentadienyl)bis[(dec-9-en-1-yl)diphenylphosphine]dimolybdenum(0)(Mo—Mo) tetrahydrofuran disolvate