The impurity elements in high -purity samples was determined by segmented scan under different pre -sputter times and different mass resolution by using GDMS VG9000.This method can effec-tively shorten the measurement time of the sample and to improve the accuracy of measurement results.%采用 VG9000型辉光放电质谱(GDMS)测定样品时,在不同预溅射时间和不同质量分辨率的情况下,对高纯样品中的杂质元素进行分段扫描测定。本法可有效的缩短样品的测定时间及提高测定结果的准确性。
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