首页> 中文期刊> 《结构化学》 >Synthesis and Crystal Structure of Ethyl2-(6-(1,3-Dioxo-4,5,6,7-tetrahydro-1H-isoindol-2(3H)-yl)-7-fluoro-3-oxo-2H-benzob1,4oxazin-4(3H)-yl) Butanoate

Synthesis and Crystal Structure of Ethyl2-(6-(1,3-Dioxo-4,5,6,7-tetrahydro-1H-isoindol-2(3H)-yl)-7-fluoro-3-oxo-2H-benzob1,4oxazin-4(3H)-yl) Butanoate

         

摘要

The title compound ethyl 2-(6-(1,3-dioxo-4,5,6,7-tetrahydro-1H-isoindol-2(3H)-yl)-7-fluoro-3-oxo-2H-benzo[b][1,4]oxazin-4(3H)-yl) butanoate 3 was synthesized by the reaction of ethyl 2-(6-amino-7-fluoro-3-oxo-2H-benzo[b][1,4]oxazin-4(3H)-yl) butanoate with 4,5,6,7-tetraydrophthalic anhydride,and its structure was determined by X-ray single-crystal diffraction.The crystal belongs to the monoclinic system,space group P21/n with a = 9.3469(2),b = 16.7715(5),c = 13.7153(4) ,β = 104.9680(10)°,μ = 0.107 mm-1,Mr = 430.42,V = 2077.08(10) 3,Z = 4,Dc = 1.376 g/cm3,F(000) = 904,T = 296(2) K,R = 0.0508 and wR = 0.1478.

著录项

  • 来源
    《结构化学》 |2009年第5期|585-589|共5页
  • 作者单位

    School of Chemistry and Biological Engineering, Changsha University of Science and Technology, Changsha, Hunan 410076, China;

    Key Laboratory of Chemical Biology and Traditional Chinese Medicine ResearchMinistry of Education of China, Hunan Normal University, Changsha 410081, China;

    Key Laboratory of Chemical Biology and Traditional Chinese Medicine ResearchMinistry of Education of China, Hunan Normal University, Changsha 410081, China;

    National Engineering Research Center for Agrochemicals, Hunan Research Institute of Chemical Industry, Changsha 410007, China;

    National Engineering Research Center for Agrochemicals, Hunan Research Institute of Chemical Industry, Changsha 410007, China;

    Department of Chemistry, University of Otago, PO Box 56, Dunedin, New Zealand;

    National Engineering Research Center for Agrochemicals, Hunan Research Institute of Chemical Industry, Changsha 410007, China;

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