The title complex [nBuSn(O)(tsglyO)]6·6CHCl3 (tsglyO=N-p-tolysulfonyl-glycinate monoanion) was syn thesized by the reaction of nBuSn(O)OH with N-p-tolysulfonyl-glycine in 1:1 molar ratio. The complex was characterized by IR, 1H NMR spectra and elemental analysis. The crystal structure was determined by X-ray diffractionmethod. It crystallizes in rhombohedral system with space group R-3. The crystal data are: a=b=2.738 7(4) nm, c= 8. The structure shows a distorted octahedral configuration with six-coordination for the central tin atom. CCDC: 274183.
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