首页> 中文期刊> 《无机化学学报》 >溶胶-凝胶法制备Ca10(PO4)6(OH)2/TiO2复合涂层及其在模拟生理体液中的行为

溶胶-凝胶法制备Ca10(PO4)6(OH)2/TiO2复合涂层及其在模拟生理体液中的行为

         

摘要

The composite films consisting of hydroxyapatite (HAP) submicron particles embedded in the gel composed of the titania nanoparticles were prepared on commercial Ti6A14V plates with titania buffer layer obtained by a spin-coating technique. The films were calcined in air at various temperatures, and the bioactivities of the films were investigated by immersing them in acellular simulated body fliud (SBF). X-ray diffraction(XRD), Fourier transform infrared spectroscopy (FTIR), Field emission-scanning electron microscopy(FESEM) and Energy dispersive X-ray (EDS) analysis were employed to investigate the phase formation and structure of the films before and after immersion, and the variations of Ca and P contents in SBF were measured by Inductively Coupled Plasma Spectroscopy(ICP). The results show that the as-prepared films were dense, homogeneous, all well-crystallized, and there was a close interracial bond between the film and the substrate. The characterisatics of the grown layer on the surfaces of the HAP/TiO2 films after immersion in SBF for different periods of time are specially discussed.

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