叠氮二乙基铝的合成及其热分解

摘要

以氯化二乙基铝(DECA)和叠氮化钠为原料合成了叠氮二乙基铝(DEAA)，报导了放大实验中遇到的问题和解决的方法,以及DEAA热分解的条件及产物。%Diethyl aluminum azide (DEAA) is synthesized by diethyl aluminum chlorode and sodoum azide. Problems arisen and methods soloved problems are reported on bench-scals research. The products and conditions of DEAA pyrolysis are also reported.