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A Microtexture Characterization of Recrystallization and Twinning in Magnesium.

机译:镁中重结晶和孪晶的微观组织表征。

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摘要

The evolution of texture and microstructure during the deformation of two Mg-based (+Al, Mn, Zn) alloys has been studied under various conditions of temperature and strain rate. The tested materials were taken from AZ31 and AM30 extruded tubes. The mechanism of recrystallization was investigated by using uniaxial compression, while twinning was studied under uniaxial tension testing. Uniaxial tension followed by annealing was also carried out in order to examine the potential of contraction and double twins for texture changes after recrystallization. Optical metallography, X-ray analysis and EBSD techniques were employed to study the texture and grain scale development.;The second part focused on the mechanisms associated with variant selection during contraction and double twinning. These twins are of practical interest since they have a high potential for texture randomization. For this purpose, magnesium alloy samples were deformed in tension at room temperature and a strain rate of 0.1s-1. The variants were characterized with respect to the orientation of the parent grain rather than of its host primary twin. This approach led to a regrouping of the 36 possible variants into 4 sets, namely the SA, SB, S C and SD, consisting of variants that are geometrically equivalent. A statistical analysis revealed that the observed secondary twins were almost entirely of the SA and SD types (misorientations of 37.5º and 69.9º, respectively). The results indicate that the formation of contraction twins and the SD type of double twins obeys Schmid's law. On the other hand, even though the SA variants are associated with significantly lower Schmid factors, they were observed to be the most common. This can be attributed to the ease of growth of this variant as well as to the very low associated accommodation strains. Similarly, the relative absence of the two other types of double twin variants (SB and SC) is explained by their geometrical configurations, which maximize the accommodation strain in the neighbouring matrix grains and minimize their potential for growth.;In the final part, the potential for decreasing the texture intensity generated during the bulk deformation of Mg alloys (AM30 and AZ31) was investigated using a combination of contraction twinning, double (secondary) twinning and static recrystallization. The results enabled the effects of initial texture and grain size on the texture and microstructural changes to be determined. A large number of twins was induced by tensile deformation at room temperature. Their volume fraction and the variants selected during straining were found to be largely responsible for the changes evident in the deformation texture. After recrystallization, most of the twin boundaries lose their character. The few that remain are contraction twins, indicating that the double twins recrystallize more rapidly. The new grains that form in the twinned regions were found to be of the order of few microns in diameter. However, these new grains do not expand into the matrix, so that the final texture is not changed significantly.;The first part of the investigation focused on the misorientations that apply to the different mechanisms of new grain formation during the hot compression of magnesium alloy AM30. This approach led to the identification of three types of microstructural features produced during deformation at high temperature (350°C at a strain rate of 0.001s-1). In the first, microbands were produced in grain interiors due to the accumulation of basal dislocations. Their orientation changes involve rotations of the basal planes to a more favorable orientation for glide, leading to geometric softening. In the second, two different types of DRX nuclei were observed, i.e. those formed i) by bulging and ii) by continuous dynamic recrystallization. Although visually distinct, the two mechanisms are formed as a result of dislocation-based processes that produce c-axis rotations toward the loading axis. The present observations indicate that new grain formation takes place in two separate stages. For low misorientation angles, the boundary character is consistent with the accumulation of basal dislocations. Once nuclei of the latter two types have formed, however, only those orientations belonging to the RD-TD fibre are able to grow. In this way, recrystallization leads to the retention of the main characteristics of the initial RD-TD texture.
机译:研究了两种Mg基(+ Al,Mn,Zn)合金在各种温度和应变速率条件下变形过程中组织和组织的演变。被测材料取自AZ31和AM30挤压管。通过单轴压缩研究了重结晶的机理,而在单轴拉伸试验下研究了孪晶。还进行了单轴拉伸,然后进行退火处理,以检查重结晶后收缩和双晶孪晶结构变化的可能性。运用光学金相,X射线分析和EBSD技术研究了织构和晶粒度的发展。第二部分着重研究了与收缩和双晶孪生过程中的变异选择有关的机制。这些双胞胎具有极大的纹理随机化潜力,因此具有实用价值。为此目的,镁合金样品在室温下的张力和0.1s-1的应变速率下变形。这些变体的特征在于母粒的方向,而不是其寄主初级双胞胎的方向。这种方法导致将36种可能的变体重新分组为4组,即SA,SB,SC和SD,它们由几何上相等的变体组成。统计分析表明,观察到的次级双胞胎几乎完全属于SA和SD类型(方向错误分别为37.5º和69.9º)。结果表明,收缩双胞胎的形成和双胞胎的SD型服从Schmid定律。另一方面,即使SA变异与较低的Schmid因子相关,也观察到它们是最常见的。这可以归因于该变体的容易生长以及相关的非常低的适应性菌株。同样,其他两种类型的双孪晶变体(SB和SC)的相对缺失也可以通过其几何构型来解释,这使相邻基质晶粒中的适应应变最大化,并使它们的生长潜力最小。利用收缩孪晶,双重(二次)孪晶和静态再结晶的组合,研究了降低镁合金(AM30和AZ31)整体变形过程中产生的织构强度的潜力。结果使得能够确定初始质地和晶粒尺寸对质地和微结构变化的影响。室温下的拉伸变形引起大量孪晶。发现它们的体积分数和在拉伸过程中选择的变体是造成变形织构明显变化的主要原因。重结晶后,大多数孪晶边界都失去了其特性。剩下的是收缩孪晶,表明孪生双晶更快地重结晶。发现在孪晶区域中形成的新晶粒的直径约为几微米。但是,这些新晶粒不会扩展到基体中,因此最终的质构不会发生明显变化。;研究的第一部分关注于镁合金热压缩过程中应用于新晶粒形成的不同机制的取向错误。 AM30。这种方法导致鉴定出在高温(350°C,应变率为0.001s-1)下变形期间产生的三种类型的微观结构特征。首先,由于基底位错的积累,在谷物内部产生了微带。它们的方向变化涉及将基面旋转到更有利于滑行的方向,从而导致几何软化。在第二个中,观察到两种不同类型的DRX核,即由i)凸起和ii)连续动态重结晶形成的。尽管在视觉上截然不同,但这两种机制是由于基于位错的过程而形成的,这些过程产生了朝向加载轴的c轴旋转。目前的观察结果表明,新的晶粒形成在两个不同的阶段发生。对于低位错角,边界特征与基底位错的累积一致。但是,一旦形成后两种类型的核,则只有属于RD-TD纤维的那些取向才能生长。这样,再结晶导致保留了初始RD-TD织构的主要特征。

著录项

  • 作者

    Martin, Etienne.;

  • 作者单位

    McGill University (Canada).;

  • 授予单位 McGill University (Canada).;
  • 学科 Engineering Mechanical.;Engineering Materials Science.;Engineering Metallurgy.
  • 学位 Ph.D.
  • 年度 2010
  • 页码 169 p.
  • 总页数 169
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

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