文摘
英文文摘
论文说明:List of Tables、List of Figures
声明
Chapter 1 Introduction
1.1.Introduction
1.1.1.Mechanism of action
1.1.2.Uses in veterinary medicine
1.2.Extraction
1.3.Analysis
1.4.Aims and objectives
Chapter 2 Separation of four sulfonamides by capillary electrophoresis
2.1.Introduction
2.2.Experimental
2.2.1.Chemicals
2.2.2.Instruments used
2.2.3.Structures of sulfonamides used
2.2.4.Standard solutions
2.2.5.Buffer composition
2.3.Results and discussion
2.3.1.Optimization of separation conditions
2.3.2.Calibration curves
2.3.3.Robustness
2.4.Summary
Chapter 3 Development of conventional sample preparation methods
3.1.Introduction
3.1.1.Solid-liquid extraction
3.1.2.Liquid-liquid extraction
3.2.Experimental
3.2.1.Sample preparation
3.3.Results and discussion
3.3.1.Protein denaturation
3.3.2.First method
3.3.3.Second method
3.3.4.Validity of analytical method
3.4.Summary
Chapter 4 Quantitative determination of sulfonamides in edible meat by SPE-CZE
4.1.Introduction
4.2.Experimental
4.2.1.Sample preparation
4.3.Results and discussion
4.3.1.Optimization of CE
4.3.2.Isolation of SAs from meat
4.3.3.Validity of analysis
4.3.4.Recovery
4.3.5.Robustness
4.3.6.Analysis of real sample
4.4.Summary
Chapter 5 Evaluation of adsorption potential of three different multiwalled carbon nanotubes for sulfonamides in edible meat
5.1.Introduction
5.2.Experimental
5.2.1.Chemicals
5.2.2.Instrumentation
5.2.3.Extraction procedure
5.3.Results and discussion
5.3.1.Adsorption study
5.3.2.Optimization of SPE procedure
5.3.3.Optimization of CE separation conditions
5.3.4.Analytical performance characteristic and recovery studies
5.4.Summary
Chapter 6 Potential of modified multiwalled carbon naotubes as solid-phase extraction adsorbent for the preconcentration of sulfonamides in edible meats
6.1.Introduction
6.2.Experimental
6.2.1.Chemicals
6.2.2.Instrumentation
6.2.3.Extraction procedure
6.3.Result and discussions
6.3.1.Stable dispersions
6.3.2.Adsorption study
6.3.3.Optimization of SPE procedure
6.3.4.Optimization of separation conditions
6.3.5.Analytical performance characteristic and recovery studies
6.4.Summary
Chapter 7 Silver Nanoparticles as adsorbent material for sulfonamides
7.1.Introduction
7.2.Experimental
7.2.1.Chemicals
7.2.2.Instrumentation
7.2.3.Synthesis of AgNPs by microwave irradiation method
7.2.4.Experiments for SAs adsorption onto AgNPs
7.3.Results and discussion
7.3.1.Possible mechanism of adsorption
7.3.2.Recovery
7.4.Future development
Chapter 8 Conclusion
8.1.Conclusions
8.2.Future studies
References
List of publications
Completed article
Acknowledgment
Biographical sketch of author
Resume of supervisor
