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Low Temperature Direct Synthesis of Strontium Titanate Powder

机译:钛酸锶粉末的低温直接合成

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Low temperature direct synthesis (LTDS) involves the preparation of a base solution of Sr~(2+), and the mixing of base solution with tetrabutyl titanate solution. LTDS is an advantageous method because it does not require the complex hydrothermal facilities and it can prevent the agglomeration in calcinations of other liquid methods. In our work, we adopted LTDS method to prepare the nano strontium titanate powders, and characterize them by XRD, FT-IR and TGA. The influences of preparation temperature and solvents on grain size and lattice parameters were investigated. The results show that preparation temperature can slightly change the lattice parameters of grain, while solvents also play important roles in the preparation.
机译:低温直接合成法(LTDS)涉及Sr〜(2+)碱溶液的制备,以及碱溶液与钛酸四丁酯溶液的混合。 LTDS是一种有利的方法,因为它不需要复杂的水热设施,并且可以防止其他液体方法在煅烧过程中发生附聚。在我们的工作中,我们采用LTDS方法制备了钛酸锶纳米粉,并通过XRD,FT-IR和TGA对其进行了表征。研究了制备温度和溶剂对晶粒尺寸和晶格参数的影响。结果表明,制备温度可以稍微改变晶粒的晶格参数,而溶剂在制备中也起着重要作用。

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