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Synthesis and characterization of novel PCA-PEG-PCA triblock copolymer

机译:新型PCA-PEG-PCA三嵌段共聚物的合成与表征

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Using chloroacetic acid(CA) and polyethylene glycol(PEG) as raw material, polyacetic acid-polyethylene glycol-polyacetic acid(PCA-PEG-PCA) triblock copolymer was synthesized by solution polycondensation. The triblock copolymer was characterized by FT-IR spectroscopy, X-Ray Diffraction and DSC. The structure of copolymer was confirmed by FT-IR. The crystallinity of compolymer was 51.24% investigated by XRD, and the result of DSC showed the PCA and PEG was homogeneous with a good compatibility.
机译:通过溶液缩聚合成使用氯代乙酸(Ca)和聚乙二醇(PEG)作为原料,聚乙酸 - 聚乙二醇 - 聚乙醇 - 聚乙酸(PCA-PEG-PCA)三嵌段共聚物合成。 三嵌段共聚物的特征在于FT-IR光谱,X射线衍射和DSC。 通过FT-IR确认共聚物的结构。 由XRD研究的复分型结晶度为51.24%,DSC的结果显示PCA和PEG具有良好的相容性。

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