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Synthesis and characterization of chitosan based silver nano composite system for antibacterial applications

机译:壳聚糖基银纳米复合体系抗菌应用的合成与表征

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An attempt has been made in the present work to Synthesize a new bio polymer (Chitosan) based Solid silver colloid nano composite system by chemical facile method. In the present research article the silver colloid was produced by chemical reduction of silver salt (silver nitrate AgNO3) solution and sodium citrate was used as a reducer. Several experimental techniques such as infrared radiation (IR), XRD, UV-Visible and FT-IR measurements were employed to characterize this bio polymer nano composite system. The IR studies confirm the salvation of Ag(0) nano particles with chitosan. UV-VIS spectrometry indicated formation of nanoparticles. The surface Plasmon resonance peak in absorption spectra of silver colloidal solution showed absorption maximum at 433 nm. Whereas XRD and FTIR studies revealed that the complexation of the host bio polymer chitosan with dispersed silver nano particles. A preliminary characteristic which allows us to realize the size of formed silver nano particles was made on the basis of the measurements of UV-VIS absorption and FT-IR. These developed films shows enhanced optical properties desired for antibacterial and biomedical applications.
机译:在本作工作中已经尝试通过化学容易法合成基于新的生物聚合物(壳聚糖)的固体银胶质纳米复合体系。在本研究制品中,通过银盐的化学还原(硝酸银酰基)溶液和柠檬酸钠作为减速器制备银胶体。采用了几种实验技术,例如红外辐射(IR),XRD,UV可见和FT-IR测量来表征该生物聚合物纳米复合体系。 IR研究证实了Ag(0)纳米颗粒与壳聚糖的救赎。 UV-Vis光谱测定表明纳米颗粒的形成。银胶体溶液吸收光谱中的表面等离子体共振峰显示出最大吸收的433nm。 XRD和FTIR的研究表明,宿主生物聚合物壳聚糖与分散的银纳米颗粒的络合。允许我们实现形成的银纳米颗粒尺寸的初步特性是基于UV-Vis吸收和FT-IR的测量来制备形成的银纳米颗粒的尺寸。这些发育薄膜显示出抗菌和生物医学应用所需的增强的光学性质。

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