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A Simple Synthesis of Silver Nanoparticles on Cellulose Paper for Antimicrobial Applications

机译:纤维素纸上的简单合成抗菌应用

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Silver nanoparticles are well known for their antimicrobial properties and have been widely used in medical and industrial applications to prevent the growth of microorganisms. The effectiveness of silver nanoparticles (AgNPs) as an antimicrobial material is influenced by their shape and size; the smaller the size, the more active the AgNPs. To prevent aggregation, the nanoparticles can be maintained by stabilizing agents. This study aims to synthesize silver nanoparticles in situ using cellulose paper and to evaluate their antimicrobial activity. For reduction of Ag~+ ions were used propane-1,2-diol. The reduction was carried out at 60, 80, and 100°C to accelerate the reaction. The formation of silver nanoparticles can be seen from the change in paper color from white to yellow or brown. This result is confirmed by the occurrence of the absorption peak in the UV-Vis spectrum between 300-500 nm. The TEM image shows the size distribution of silver nanoparticles affected by their reduction temperature. Antimicrobial tests provide a clear zone from the bottom of the paper to the edge. The reaction temperature at 60°C showed the best antimicrobial activity with AgNPs averaging at 6 nm. This method can be applied to antimicrobial paper preparation with controlled size and distribution.
机译:银纳米粒子均以其抗微生物性质众所周知,已广泛用于医疗和工业应用中以防止微生物的生长。银纳米颗粒(AgNP)作为抗微生物材料的有效性受其形状和尺寸的影响;尺寸越小,AGNPS越活跃。为了防止聚集,可以通过稳定剂维持纳米颗粒。本研究旨在使用纤维素纸对原位合成银纳米颗粒,并评估其抗微生物活性。用于减少Ag〜+离子的丙烷-1,2-二醇。将还原在60,80和100℃下进行以加速反应。从纸张颜色的变化可以从白色到黄色或棕色的变化中看到银纳米颗粒的形成。通过300-500nm之间的UV-Vis光谱中的吸收峰的发生来证实该结果。 TEM图像显示通过还原温度影响的银纳米粒子的尺寸分布。抗微生物检验从纸张底部提供清晰的区域到边缘。 60℃的反应温度显示最佳的抗微生物活性,其agnps平均在6nm处。该方法可以应用于具有受控尺寸和分布的抗微生物纸制剂。

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