Preparation of CNTs-supported Fe3O4 and Fe3C Nano-particles and the Investigation on their Magnetic Properties

摘要

Magnetite (Fe₃O₄) nanoparticles uniformly loaded on multi-walled carbon nanotubes (MWCNTs) were synthesized by a wet chemistry method, and then carbon coated Fe₃C nanoparticles supported by MWCNTs were prepared by heat-treatments subsequently in nitrogen at 600 degC and in acetylene atmosphere at 500 degC. The as-prepared nanoparticles were all single crystals with a size distribution ranging from 10 to 60nm upon TEM and XRD measurements. The magnetic properties of these two kinds of nanoparticles were measured using vibrating sample magnetometer (VSM) at room temperature. The results show that above materials are useful for magnetic materials, and the method to produce magnetic nanoparticles coated with graphite is rather simple