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Nanostructures of tin oxide by a simple chemical route: synthesis and characterization

机译:简单化学途径氧化锡纳米结构:合成与表征

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Tin oxide (SnO_2) nanostructures have been synthesized by a simple chemical route. The morphology and crystallization of the samples can be controlled by changing the mixed solution of tin chloride. The precursors were calcined at 600 °C for 2 h in air to obtain the SnO_2 nanorods and nanoparticles. The phase composition of the samples was investigated by XRD and electron diffraction analysis. The results confirmed the formation of a SnO_2 phase with tetragonal structure. The optical properties of the nanostructures were investigated by UV-vis spectroscopy. The estimated band gaps of nanorods and nanoparticles were 3.39 and 4.23 eV, respectively. The results revealed that the morphologies and band gaps of the samples varied with the mixed solution of tin chloride.
机译:通过简单的化学途径合成氧化锡(SnO_2)纳米结构。 可以通过改变氯化锡的混合溶液来控制样品的形态和结晶。 将前体在600℃下在空气中煅烧2小时,得到SnO_2纳米棒和纳米颗粒。 通过XRD和电子衍射分析研究样品的相组成。 结果证实了具有四边形结构的SnO_2相的形成。 通过UV-Vis光谱研究纳米结构的光学性质。 纳米棒和纳米颗粒的估计带间隙分别为3.39和4.23eV。 结果表明,样品的形态和带间隙随着氯化锡的混合溶液而变化。

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