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Synthesis of nanorod structured polyaniline nanofiber for high electrochemical efficiency

机译:高电化学效率的纳米棒结构聚苯胺纳米纤维的合成

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Synthesis of polyaniline (PANI) nanofiber via interfacial polymerization method with ammonium peroxy-disulfate (APS) used as a initiator catalytic agent, aniline&APS molar concentration as a key factor to produce nanofiber without any anionic or cationic surfactant. The optical property of PANI nanofiber was studied by UV-Visible spectroscopy and the obtained absorption peaks around 353 and 634nm. Surface morphology of PANI nanofiber carried by Field emission scanning electron microscopy which gives nanofiber diameter is below 20nm, and Fourier-transform infrared (FTIR) spectra for chemical functional groups. Electrochemical measurement was performed by cyclic voltammetry (CV) and Linear sweep voltammetry (LSV), they shows the high current rate in anodic and cathodic peaks represents high electrochemical property.
机译:通过界面聚合方法合成聚苯胺(PANI)纳米纤维用界面聚合方法用作引发剂催化剂,苯胺和APS摩尔浓度作为生产纳米纤维而没有任何阴离子或阳离子表面活性剂的关键因素。 通过UV可见光谱研究PANI纳米纤维的光学性质,并获得353和634nm的获得的吸收峰。 PANI纳米纤维的表面形态由现场发射扫描电子显微镜携带,其给予纳米纤维直径低于20nm,以及用于化学官能团的傅里叶变换红外(FTIR)光谱。 通过循环伏安法(CV)和线性扫描伏安法(LSV)进行电化学测量,它们显示出阳极和阴极峰中的高电流率代表高电化学性能。

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