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Synthesis and Characterization of MWCNT/Dolomite Hybrid Compound as Potential Composite Fillers

机译:MWCNT /白云石杂交化合物作为潜在复合填料的合成与表征

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Multiwalled carbon nanotubes/dolomite (MWCNT/dolomite) hybrid compound was synthesized using the Chemical Vapour Deposition (CVD) technique. The catalyst was prepared via the co-precipitation method. The press involves the drying of the precipitate followed by calcination at 900°C. Upon completion of calcinations press, the reduction press was carried under H_2 at 400°C and growth in a CH_4/N_2 gas mixture at 800°C for 30 minutes The reduction press was carried out under H_2 and growth in a CH_4/N_2 gas mixture at 800°C for 30 minutes. The morphological assessment using Field Emission Scanning Electron Microscope (FESEM) showed that the CNT was successfully grown on dolomite particle. High Resolution Transmission Electron Microscope (HRTEM) micrograph further confirmed the presence of MWCNT with varied length and geometry on dolomite surfaces, supported the formation of MWCNT on the dolomite's particle.
机译:使用化学气相沉积(CVD)技术合成多壁碳纳米管/白云石(MWCNT / Dolomite)杂化化合物。通过共沉淀法制备催化剂。压力机涉及沉淀干燥,然后在900℃下进行煅烧。在完成煅烧时,将还原压榨机在400℃下在400℃下携带,并且在800℃下在800℃下生长30分钟,减少压力机在H_2下进行,并在CH_4 / N_2气体混合物中进行生长。在800℃下30分钟。使用场发射扫描电子显微镜(FESEM)的形态学评估显示CNT在白云石颗粒上成功生长。高分辨率透射电子显微镜(HRTEM)显微照片进一步证实了在白云石表面上具有不同长度和几何形状的MWCNT的存在,支持在白云石颗粒上形成MWCNT。

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