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Fabrication and characterization of multi-walled carbon nanotube for conductive polymer composite

机译:多壁碳纳米管用于导电聚合物复合材料的制造与表征

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Dry surface electrocardiogram electrode that gives the flexibility and conductivity have been studied before by other researchers using conductive polymer composite. This paper presents the development of Multiwalled Carbon Nanotube (MWCNT) as filler and Polydimethylsiloxane (PDMS) as polymer matrix. Solution mixing has been used to synthesize the MWCNT in Isopropyl Alcohol (IPA) for better dispersion before combining with PDMS which then the mixture were poured into mold. To investigate the material and electrical properties of polymer composite fabricated electrode, Raman Spectroscopy Analysis was used. It was found that, the Raman band for fabricated electrodes have peaks at D-band (1351 cm~(-1)), G-band (1593 cm~(-1)) but there was no peak at 2D-band. This Raman Spectroscopy also being measured for MWCNT powder and pure PDMS in order to distinguish the shape of Raman Graph. From the results obtained, the MWCNT/PDMS composite electrode shows similar shape to pure PDMS Raman spectrum. This indicates the fabricated electrode is not conductive and more inclined towards insulating properties. The electrical test conforms well to the Raman results which shows non-conductive behavior. Further studies need to be executed to determine the optimized weight ratio between MWCNT and PDMS.
机译:使用导电聚合物复合材料的其他研究人员之前研究了给予柔韧性和电导率的干燥表面心电图电极。本文介绍了多壁碳纳米管(MWCNT)作为填料和聚二甲基硅氧烷(PDMS)作为聚合物基质的发展。溶液混合已被用于在异丙醇(IPA)中合成MWCNT,以便在与PDM组合之前更好的分散体,然后将混合物倒入模具中。为了研究聚合物复合材料的材料和电性能,使用拉曼光谱分析。发现,用于制造电极的拉曼带在D波段(1351cm〜(-1)),G波段(1593cm〜(-1)),但在2D波段中没有峰。该拉曼光谱还针对MWCNT粉末和纯PDMS测量,以区分拉曼图的形状。从获得的结果,MWCNT / PDMS复合电极显示出与纯PDMS拉曼光谱相似的形状。这表明制造的电极不导电并且朝向绝缘性能倾斜。电气测试符合显示出显示非导电行为的拉曼结果。需要进行进一步的研究以确定MWCNT和PDMS之间的优化重量比。

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