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Preparation of iron tailings glass-ceramics by sol-gel method

机译:用溶胶 - 凝胶法制备铁尾矿玻璃陶瓷

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For the preparation of glass-ceramics by iron tailings, the sintering and melting methods have been used in the past, but the two methods are short of high energy consumption. In this test, the sol-gel method has been adopted. Because the sol-gel method requires high purity to prepare raw materials, and there are many impurities in iron tailings, which is inconsistent with the preparation requirements of sol-gel method. Therefore, in this experiment, useful elements in iron tailings were extracted. Iron tailings were obtained by thermal-alkali reaction, and Fe was obtained by acid reaction, so as to prepare Ca-Mg-Al-Si system glass-ceramics. After the preparation of sol-gel, the basic glass was obtained, and after nucleation and crystallization, the microcrystalline glass whose main phase was diopside was obtained.
机译:通过铁尾矿制备玻璃陶瓷,过去使用了烧结和熔化方法,但这两种方法缺乏高能耗。在该试验中,已采用溶胶 - 凝胶法。因为溶胶 - 凝胶法需要高纯度来制备原料,并且铁尾矿中有许多杂质,这与溶胶 - 凝胶法的制备要求不一致。因此,在该实验中,提取铁尾矿中的有用元素。通过热碱反应获得铁尾,通过酸反应获得Fe,以制备Ca-Mg-Al-Si系统玻璃陶瓷。在制备溶胶 - 凝胶后,获得碱性玻璃,并在成核和结晶后,获得主相是偶氮的微晶玻璃。

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