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The characterization of ceramic alumina prepared by using additive glass beads

机译:用添加剂玻璃珠制备陶瓷氧化铝的表征

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The ceramic alumina has been made by using additive glass bead (5 and 10 % wt.). There are two kinds of materials, such as : gamma Alumina and glass bead. Synthesis of alumina was done by ball milling for 24 hours, then the mixed powder was dried in drying oven at 100 °C for 6 hours. Furthermore, the dried powder was mixed by using 2 % of PVA and continued with compacted to form a pellet with pressure of 50 MPA. The next step is sintering process with variation temperature of 1150, 1200, 1250, 1300 and 1400 °C and holding time for 2 hours. The characterization conducted are consist of test density, hardness, shrinkage, and microstructure. The results show that ceramic alumina with addition of 10 % wt. glass bead has the higher value of density, hardness and shrinkage than addition of 5% wt. glass bead. The highest characterization of ceramic alumina with addition 10 % glass bead was achieved at sintering temperature of 1400 °C with density 3.68 g/cm~3, hardness vickers 780.40 Hv and shrinkage 15.23 %. The XRD results show that it was founds a corrundum (alpha Alumina) as dominant phase and mullite as minor phase.
机译:通过使用添加剂玻璃珠(5和10%重量)制备陶瓷氧化铝。有两种材料,如:γ氧化铝和玻璃珠。氧化铝的合成通过球磨24小时完成,然后将混合粉末在100℃下干燥烘箱6小时。此外,通过使用2%的PVA混合干燥的粉末并继续压实以形成具有50MPa的压力的沉淀。下一步是烧结过程,变化温度为1150,1200,1250,1300和1400℃并保持时间2小时。所进行的表征由测试密度,硬度,收缩和微观结构组成。结果表明,陶瓷氧化铝加入10%wt。玻璃珠具有较高的密度,硬度和收缩值,而不是加入5%wt。玻璃珠。在1400℃的烧结温度下达到10%玻璃珠的陶瓷氧化铝的最高表征,密度为3.68g / cm〜3,硬度维氏780.40室温和收缩15.23%。 XRD结果表明,它被发现是占主导地相和莫来石的钙(alpha氧化铝)。

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