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Production of Fatty Acid Methyl Ester from Low Grade Palm Oil Using Eutectic Solvent Based on Benzyltrimethylammonium Chloride

机译:基于苄基三甲基氯化铵的共晶溶剂,使用共晶溶剂从低级棕榈油生产脂肪酸甲酯

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In this study, high content of free fatty acid (FFA) from low grade palm oil (LGPO) was treated using deep eutectic solvent (DES). This DES was prepared via mixing of p-toluenesulfonic acid monohydrate (PTSA) with benzyltrimethylammonium chloride (BAC). Various effect of reaction conditions were studied such as catalyst dosage (0.5% to 4.5%), molar ratio (2:1 to 12:1), reaction time (10 to 120 min) and reaction temperature (30 °C to 80 °C). This study exhibited that 2% catalyst dosage, 10:1 molar ratio of methanol to oil, 30 min of reaction time and reaction temperature of 60 °C were the optimum condition to reduce the FFA content to less than 2%.
机译:在该研究中,使用深共晶溶剂(DES)处理来自低级棕榈油(LGPO)的高含量的游离脂肪酸(FFA)。通过将对甲苯磺酸一水合物(PTSA)与苄基三甲基氯化铵(BAC)混合制备该DES。研究了反应条件的各种影响,例如催化剂剂量(0.5%至4.5%),摩尔比(2:1至12:1),反应时间(10至120分钟)和反应温度(30℃至80℃) )。该研究表现出2%催化剂剂量,10:1甲醇与油的摩尔比,反应时间30分钟和60℃的反应温度是将FFA含量降低至小于2%的最佳条件。

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