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Synthesis of Aluminium Nanoparticles in A Water/Polyethylene Glycol Mixed Solvent using u-EDM

机译:用U-EDM在水/聚乙二醇混合溶剂中合成铝纳米粒子

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Nanoparticles present a practical way of retaining the results of the property at the atomic or molecular level. Due to the recent use of nanoparticles in scientific, industrial and medical applications, synthesis of nanoparticles and their characterization have become considerably important. Currently, aluminium nanoparticles have attracted significant research attention because of their reasonable cost, unique properties and interdisciplinary emerging applications. The present paper reports the synthesis of aluminium nanoparticles in the mixture of Deionized water (DI water) and Polyethylene Glycol (PEG) using a developed micro-Electrical Discharge Machining (u-EDM) method. PEG was used as a stabilizer to prevent nanoparticles from agglomeration produced during the u-EDM process. The synthesized aluminium nanoparticles were examined by Transmission Electron Microscopy (TEM), Energy Dispersive Analysis by X-rays (EDAX) and Selected Area Electron Diffraction (SAED) pattern to determine their size, shape, chemical nature and crystal structure. The average size of the polyhedral aluminium nanoparticles is found to be 196 nm.
机译:纳米颗粒呈现了在原子或分子水平处保留性质结果的实用方法。由于最近在科学,工业和医疗应用中使用纳米颗粒,纳米颗粒的合成及其表征已经变得相当重要。目前,铝纳米粒子由于其合理的成本,独特的特性和跨学科新兴应用而引起了显着的研究。本文用发育的微电放电加工(U-EDM)方法报道了在去离子水(DI水)和聚乙二醇(PEG)的混合物中合成铝纳米粒子。 PEG用作稳定剂以防止在U-EDM过程中产生的纳米颗粒。通过透射电子显微镜(TEM)检查合成的铝纳米粒子,通过X射线(edax)和选择的区域电子衍射(SAED)图案来确定其尺寸,形状,化学性质和晶体结构。发现多面体铝纳米粒子的平均尺寸为196nm。

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